C12 - Testing substances Flashcards

1
Q

test for hydrogen = positive

A

lighted splint pops

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2
Q

test for o2 = positive

A

a glowing splint relights

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3
Q

test fro co2

A

turns limewater milky

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4
Q

test for chlorine

A

damp blue litmus paper turns white (bleaches)

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5
Q

flame tests process

A

-nichrome wire loop dipped into concentrated HCL to clean it
-dipped into HCL + metal compound
-hold loop in blue bunsen burner flame
-colour = identifies metal ion

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6
Q

flame tests

A

identifies metal ion by colour of flame

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7
Q

mixture of metal ions in flame test

A

colours can be masked

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8
Q

Li+ flame colour

A

crimson

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9
Q

Na+ flame colour

A

yellow

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10
Q

K+ flame colour

A

lilac

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11
Q

flame colour of Ca2+

A

orange - red

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12
Q

Cu2+ flame colour

A

green

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13
Q

Mg2+ flame colour

A

no colour

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14
Q

metal cation test is with

A

sodium hydroxide

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15
Q

metal cation test with sodium hydroxide test

A

identifies metal positive ions in unknown compound

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16
Q

metal cation test with sodium hydroxide for aluminium, calcium, magnesium

A

white precipitate

17
Q

metal cation test with sodium hydroxide - aluminium

A

precipitate will dissolve

18
Q

metal cation test with sodium hydroxide test - mg and ca

A

precipitate will not dissolve
-then can be distinguished with a flame test

19
Q

copper II ions colour precipitate

A

blue

20
Q

iron II ions colour precipitate

A

green

21
Q

iron III ions colour precipitate

A

brown

22
Q

testing for carbonate

A

fizzing + co2 produced
-when dilute acid is dded

23
Q

group 1 carbonates

A

soluble whereas most aren’t

24
Q

Halide test

A

add dilute nitric acid and silver nitrate solution
-if a precipitate forms = present

25
Q

halide test - why add nitric acid

A

-to dissolve compound and remove carbonate ions
-prevents a precipitate forming with silver ions + carbonate and interfere with the test

26
Q

halide colour precipitate

A

I = yellow
Cl = white
Br = cream

27
Q

sulfate test

A

-add dilute HCL and barium chloride solution

28
Q

sulfate test - why add HCL

A

removes carbonate ions to precipitatae doesn’t form with barium ions

29
Q

sulfate test present

A

-white precipitate
-this is insoluble barium sulfate

30
Q

modern instrumental pros

A

-highly accurate
-sensitive
-quicker
-allow small samples to be analysed

31
Q

cons of modern instruments

A

-expensive
-special training
-only interpreted by comparing to known substances

32
Q

flame emission spectroscopy

A

-analyse samples for metal ions

33
Q

flame emission spectroscopy process

A

-sample is heated in a flame
-energy provided excites electrons in metal ions
-allows them o jump to higher energy levels
-when they fall back to lower levels = energy is released as light

34
Q

spectrometer

A

wavelengths of light produced can be analysed by passing through this

35
Q

spectrometer - metal ions

A

-each type absorbs/emits its own line spectrum

36
Q

line spectrum

A

own characteristic pattern of radiation
-identifies metal ions by comparing to a database on a computer

37
Q

spectrometer on concentration

A

-measures intensity of light with a specific wavelength of a particular metal ion
-machine is calibrated sing known concentrations to give a value

38
Q

spectrometer pros

A

-provide accurate ways to monitor water for metal ions

39
Q

spectrometer used in

A

steel industry
-controls trace metals present = quality