Purification Flashcards

1
Q

To separate sublimated compounds from non sublimable impurities which technique is used

A

Sublimation

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2
Q

Which technique is based on diffrence in solubility of the compound and impurities

A

Crystallization

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3
Q

Technique used to separate volatile components from non volatile impurities

A

Distillation

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4
Q

Technique used to separate liquids having sufficient diffrence in their boiling point

A

Distillation

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5
Q

Technique used when diffrence in boiling point of the compounds is not much

A

Fractional distillation

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6
Q

Each successive Condensation and vaporization unit in fractionation column is called

A

Theoretical plate

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7
Q

The technique used to remove substance which are steam volatile and immiscible with water

A

Steam distillation

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8
Q

An example of steam distillation is

A

Anneline water mix

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9
Q

Diffrential Extraction is carried out in

A

Separatory funnel

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10
Q

commonly used absorbent are

A

Silica gel and alumina

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11
Q

The types of adsorption chromatography is

A

Coloumn chromatography and thin layer chromatography

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12
Q

Ninhydrin is used for detection of

A

Amino acids

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13
Q

Stationary phase in paperchromatogaphy is

A

Water trapped in chromatogram paper

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14
Q

Paper chromatography is a type of

A

Partition chromatography

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15
Q

Carbon and hydrogen are detected by heating the component with

A

Copper(II) oxide

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16
Q

Why is sodium metal used in lassaignes test

A

To convert covalent form into Ionic form

17
Q

The oxidation state of Outer Fe in Prussian blue is

A

3

18
Q

The oxidation state of inner Fe in Prussian blue is

A

2

19
Q

Hexacyanido ferrate is

A

Fe4[ Fe (CN)6]3

20
Q

For testing of Sulphur we treat the sodium fusion extract with sodium nitroprusside

A

[ Fe(CN)5 NOS ]4- ( violet colour)

21
Q

Blood red sodium thiocyanate is

A

[ Fe (SCN)] 2+

22
Q

If Excess sodium is used the thiocyanate will

A

Decomposes to yield Cyanide and sulphide

23
Q

The formula of ammonium phosphomolybdate is

A

(NH4)3 PO4 .12 MoO3 [Yellow ppt]

24
Q
A