Test Methods Flashcards

1
Q

Wash vials are made up of your

A

Sample diluent

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2
Q

Nir test products

A

OXY
PMS
HBT

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3
Q

wash vials in GC are usually the

A

diluent

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4
Q

Processing width area intuition

A

These look pretty straightforward to understand. Anything below that area or height won’t be considered a peak.
Example:

If we raise the minimun peak area to 230:

Same thing for the peak height, as we can see its 58 but if we make it 61 we remove that peak.

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5
Q

When in COP nothing shows up in the sample, (it looks like a water blank)

A

You report it as less than your LOQ which is 1.1 ppm for equipco

If something shows up you report that number.

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6
Q

When reviewing your empower run always 2 mistakes you made previously

A

Make sure that your processing method matches

And use the initial SS form the show all Columns.

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7
Q

remember when putting LOD dishes in the oven to

A

keep the lid slightly off

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8
Q

GC Instrument setup important points

A
  • Septum finger tight
  • correct syringe size (make sure it’s in the needle seat it’s smooth)
  • wash vials and your waste vials
  • column that it is the right One, it is also etched
  • gases and hydrogen generator
  • do not turn off the flow without turning of the temperature
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9
Q

oxy 512 2 sample

A
dry 
(1)NIR
(2) IM
Single mill pass
IM
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10
Q

When filling in a the COp paper worksheet.

A

“Results as “ this is circled in the paper

Mar limit

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11
Q

nCOB worksheets

A

5224

Retain

LOD 3 hours

Assay by LC

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12
Q

how to measure size of particles in the microscope software

A

hold control and drag for particle size

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13
Q

Tell me 2 things you need to check when doing GC gabe empower not setting up

A
  • grey buttons down back injector -> injection volume
  • config a little bit highr thatn the grey button, it’s the grey button to the left, go down to back injector hit enter, go down and check  check syringe size
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14
Q

Rachel Morris empower truck

A

Select your sample set or results sets right click view as processing method.

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15
Q

What vials are used for hplc impurities ?

A

Polypropylene

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16
Q

1200 HPLC are used only for

A

COP

17
Q

blank weight and volume KF

A

50 micro liters, 0.05g

18
Q

SOP fro trending

A

11613

19
Q

Codeine Phosphate, USP Worksheet B

A

FRM-32447

There are two grades coarse grade and standard grade. If standard section 3.0 is not applicable.

DS-TMD-5222

(1) KF
(2) IMP by HPLC
(3) particle size by ATm

20
Q

Pms finals labels special detail

A

Lowe case

21
Q

If your unsure where something in your chrome could me coming from

A

Run a zero volume injection, maybe a blank or DI water on GC

22
Q

CMB5 and npma reporting assay in SAP

A

CMB5 dry wet wet aim is wet

Npma dry dry wet aim is the only wet