Mistakes Flashcards
most investigations according to gabriel are related to what to tests
assays and impurities and IM
Clean and organized work areas are positive because
Reduce cross cont
Reduce error
Respect the next analyst
Reagents and solvents exp date
Date on manufactured bottle coa
NIR Mistake before login on
To the computer
Make sure you are using the right instrument in the instrument selector.
Remember Shannon mistake documention correction on the retain
Should read (correct sample ID)
Accidentally hit print with incorrect decimal places
Review pH procedure
Calibrate, and check buffers they must be within 0.03.
hplc maintenance sop
11360 major minor repairs
moisture check anakyzers
sensitivity injection
measure instument response on very low concentations
ANSI stands for
American national standard institute
Bill takeaway 2
It is what it is
100.0% confidence
Difference between analyst and a good analyst
nPOB1 and nPOB2
next generation purified oxycodone base step 1
Micronized is only from
athens
Zachary ferrule why does it exist and how to make it?
It exist so that the Column attaches with out falling. The fitting must slide freely but not fall.
Twist once. And then tighten and untighten with wrench.
Mural
King of sweden swweede landing
nCOB stands for
next generation crude oxycodone base
Nothing with data goes in trash
Shredder
Types of solutions for ph
Storage solutions and filling solutions
Documents to check when receing tankers and what to check on them
- COA
- BO Lading
- Wash Certificate must be signed
(Sometimes it ifs dedicated it might not come with it)(sodium hydroxide with letter of dedication)
Check that they are initial and date and batch from someone from the warehouse
When trying to focus in on the global IM microscope part
Use top light and start at 5x
how do you know the tapes need to be reloeaded?
you get the pink
Glassware washing 3 steps —- pipettes
Acero acid, tap and DI water — tip up, column rinsing wait when the water level is down, tip down on furnaces
Safety always card in and out buttons and exitinguesrs
Panic button medical alert buttons
Extra details when washing pipets Shannon
Pop 2 pills and leave 3 hours rinsing
Then dry 3 hours tip down
Zach ask questions
As i go
oven purge instruccions
BEFORE TURNING OFF make sure
turn on pump, open line, slight purge 20 to 25 mg somethings
you pay attention if other people are running stuff
How to dispose of a reagent
it has a CH sticker
- non controlled moved
- disposed two boxes on the right
- flush the container with water
- cross out with a sharpie throw in the trash
What to remember about the plug in ph
Plug when not In use unplug when in use
get used to calibration decimal and units checking
-
Waste inventory spreadsheet zach
Departments EHS waste inventory make sure its in Wilmington
COM
crude oxymorphone
What is used to decolor powders ?
Loose carbon or encapsulated carbon
Production should put the —- weight on the bag
Tate
HM I S
Health materials identification system
Dial number emergency
55
Where are the stock stds in the safe from?
They buy no USP stds they make theyre own jn athens.
IOP stands for
instrument operating procedure
Roi stands for
Residue on ignition
Whats in the safe?
Retains disposal stock stds
Whenever you sign as a witness you share in the — remember you can
Responsibility remember you can always decline.
Micro cal and bulk calibration due
Micro every 3 months bulk every 6
Raw materials that are received could be either two things
And what do yo do with them after you receive them
Label checks or raw materials in jars with green lids to be tested
Whenever they’re received they’re immediately disposed
KF Equation detail you didn’t know
ml * KF factor / weight of sample
FG acronym
Fine grade
- 04
- 06
What is that? Bill asked
It means nothing without any units.
on the LOP SOP it says about 30 minutes accordig to danielle it should be
NLT then 30 min
PM Is what
Preventive maintenance
nPHB
next generation purified hydrocodone base
Remember I just don’t work with APIs I work with —– Edwin
Narcotics
where are the tubes used in comparison
S2-3
What is CAPA?
Corrective action preventive action.
Audit trails
Are a reconstruction of how the batch came to be
Think about training validation was it cleaned.
Orion 3 ph Jackie didn’t know how to change from mV to ph
Justin had to come and press down.
Difference between environmental impact an element
An element is something which can be impacted
Danielle NIR out of what range
Always check the calibration range
20/20/20vision rule
Use the 20-20-20 rule. Every 20 minutes, take a 20-second break and focus your eyes on something at least 20 feet away.
— g of tolerance , how much for weight cakes
0.3 g 1%
Of how much
Special detail Shannon taught you about the NIR
Put the sample as soon as you get to the area
It its an old tanker lot if wont bring
A COA
What is the bill of lading?
Check MFG and disctributor adress this is used to determined reduced or full testing
Make sure its legible
Chain of custody bill meeting
Always check in and out
crude vs next generation
crude is like with impurities
next genertaion
When doing the balances don’t write the —-!!
Units. It’s usually included.
Appearance EC
Fill in the circles, if it tells you to write it, you should always choose white or white off not both.
What would be a considered as metallic particle
Anything silver or shiny.
Just remember tepentadol gets
CE
The two big balances are called —
Pan
How do i know the tolerances for each balances ? What about the weight set?
SOP fot the olerances. The actual weights change when the weight set changes.
raman sample holders
vial holder nose cone (this is used directly against the sample container)
according to game stress before cleanup reduces
downtime
fLOD procedure
fLOD Halogen moisture Balance training EC 11-28-16
remember on/off button, tare button, open/close button (last 24 hours, this calibration has no print out )
method button to choose the material or product hit enter
code button to enter sample info
c1 sample a-z letter to switch to alphabet up down arrow c2 batch c3 extra info keep hitting code until I come to the home screen
print out and compare to table
add sample spread it
hit start
wet wight is my weight
nATA stans for
nxt generation anhydrous thebaine alkaloid
when writing a bought mfg chemical write
MFG, lot no
Mental conflation. Non routines va non controlled
It is obvious
when to accept non routine samples?
SA, PR # or a CoC
Noncoformqnces types
Events
Deviations
Events -(ICMS)
Bill meeting When an auditor comes to check all documents what is this called
Audit trail
dad detector
diode array detector
The main reason for this is that a DAD/PDA can always be set to scan a range of all probable wavelengths, but a single (or multi-wavelength) detector can not.
Phone interview
Exited introductions meting new people
Mobile phase filters
0.45 micron MP
remmebr to fill forrest zach
departmetns –> wilimgnton –> enviromental –>wast inventory
departmetns –> wilimgnton –> hazard communication–> sds
Retain Shannon mistake weighing
Always make sure it is in the right decimal place.
finished product is the only one with —- retain date eveything else that goes on the —- gets 1
finished gets 6 year, eveything else in the green lid jar gets 1 year
ICMS
Instrument calibration maintenance system
Instrument Calibration & Maintenance System (ICMS) is a convenient way to maintain all your records on the equipment, machinery, instrumentation, and very much all of your company assets. Supplied as a separate product or as an integrated part of any Matrix Gemini modules, it holds and reports on any important information. ICMS tracks all your assets, starting from installation, maintenance, repairs, calibration until the disposal of any unusable assets.
How to turn off vacuum LOD
Turn off punk first then the valve the release the pressure
Where are the frops planted ? And what are they called
Tazmania poppy seeds
DOT
Department of transportation
Remind yourself of the button to change units in the balances and digits on the pH
-
Choose what when choosing NIR results
Measurement done:
Excel keep paswrod
For passweod
watch for the double negative in the
NAOH tanker
Product flow chart
RM->Wet ->Dry->Mill?->Finishing?
Spec says <0.10%
Your results are 0.0045% how should you report it
0.005% always report something
What’s the difference between an analyst and good analyst ?
Analyst produces results and a good analyst ask if it makes sense
Post it notes 3 bill
Do I understand what they’re asking ?
Do I owe it?
Do I agree?
Read well. What about the sample?
Is it dried or wet
