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philip > Mistakes > Flashcards

Mistakes Flashcards

1
Q

most investigations according to gabriel are related to what to tests

A

assays and impurities and IM

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2
Q

Clean and organized work areas are positive because

A

Reduce cross cont
Reduce error
Respect the next analyst

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3
Q

Reagents and solvents exp date

A

Date on manufactured bottle coa

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4
Q

NIR Mistake before login on

To the computer

A

Make sure you are using the right instrument in the instrument selector.

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5
Q

Remember Shannon mistake documention correction on the retain

A

Should read (correct sample ID)

Accidentally hit print with incorrect decimal places

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6
Q

Review pH procedure

A

Calibrate, and check buffers they must be within 0.03.

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7
Q

hplc maintenance sop

A

11360 major minor repairs

moisture check anakyzers

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8
Q

sensitivity injection

A

measure instument response on very low concentations

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9
Q

ANSI stands for

A

American national standard institute

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10
Q

Bill takeaway 2

A

It is what it is

100.0% confidence

Difference between analyst and a good analyst

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11
Q

nPOB1 and nPOB2

A

next generation purified oxycodone base step 1

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12
Q

Micronized is only from

A

athens

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13
Q

Zachary ferrule why does it exist and how to make it?

A

It exist so that the Column attaches with out falling. The fitting must slide freely but not fall.

Twist once. And then tighten and untighten with wrench.

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14
Q

Mural

A

King of sweden swweede landing

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15
Q

nCOB stands for

A

next generation crude oxycodone base

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16
Q

Nothing with data goes in trash

A

Shredder

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17
Q

Types of solutions for ph

A

Storage solutions and filling solutions

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18
Q

Documents to check when receing tankers and what to check on them

A
  • COA
  • BO Lading
  • Wash Certificate must be signed

(Sometimes it ifs dedicated it might not come with it)(sodium hydroxide with letter of dedication)

Check that they are initial and date and batch from someone from the warehouse

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19
Q

When trying to focus in on the global IM microscope part

A

Use top light and start at 5x

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20
Q

how do you know the tapes need to be reloeaded?

A

you get the pink

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21
Q

Glassware washing 3 steps —- pipettes

A

Acero acid, tap and DI water — tip up, column rinsing wait when the water level is down, tip down on furnaces

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22
Q

Safety always card in and out buttons and exitinguesrs

A

Panic button medical alert buttons

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23
Q

Extra details when washing pipets Shannon

A

Pop 2 pills and leave 3 hours rinsing

Then dry 3 hours tip down

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24
Q

Zach ask questions

A

As i go

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25
Q

oven purge instruccions

BEFORE TURNING OFF make sure

A

turn on pump, open line, slight purge 20 to 25 mg somethings

you pay attention if other people are running stuff

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26
Q

How to dispose of a reagent

A

it has a CH sticker

  • non controlled moved
  • disposed two boxes on the right
  • flush the container with water
  • cross out with a sharpie throw in the trash
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27
Q

What to remember about the plug in ph

A

Plug when not In use unplug when in use

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28
Q

get used to calibration decimal and units checking

A

-

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29
Q

Waste inventory spreadsheet zach

A

Departments EHS waste inventory make sure its in Wilmington

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30
Q

COM

A

crude oxymorphone

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31
Q

What is used to decolor powders ?

A

Loose carbon or encapsulated carbon

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32
Q

Production should put the —- weight on the bag

A

Tate

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33
Q

HM I S

A

Health materials identification system

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34
Q

Dial number emergency

A

55

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35
Q

Where are the stock stds in the safe from?

A

They buy no USP stds they make theyre own jn athens.

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36
Q

IOP stands for

A

instrument operating procedure

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37
Q

Roi stands for

A

Residue on ignition

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38
Q

Whats in the safe?

A

Retains disposal stock stds

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39
Q

Whenever you sign as a witness you share in the — remember you can

A

Responsibility remember you can always decline.

40
Q

Micro cal and bulk calibration due

A

Micro every 3 months bulk every 6

41
Q

Raw materials that are received could be either two things

And what do yo do with them after you receive them

A

Label checks or raw materials in jars with green lids to be tested

Whenever they’re received they’re immediately disposed

42
Q

KF Equation detail you didn’t know

A

ml * KF factor / weight of sample

43
Q

FG acronym

A

Fine grade

44
Q
  1. 04
  2. 06

What is that? Bill asked

A

It means nothing without any units.

45
Q

on the LOP SOP it says about 30 minutes accordig to danielle it should be

A

NLT then 30 min

46
Q

PM Is what

A

Preventive maintenance

47
Q

nPHB

A

next generation purified hydrocodone base

48
Q

Remember I just don’t work with APIs I work with —– Edwin

A

Narcotics

49
Q

where are the tubes used in comparison

A

S2-3

50
Q

What is CAPA?

A

Corrective action preventive action.

51
Q

Audit trails

A

Are a reconstruction of how the batch came to be

Think about training validation was it cleaned.

52
Q

Orion 3 ph Jackie didn’t know how to change from mV to ph

A

Justin had to come and press down.

53
Q

Difference between environmental impact an element

A

An element is something which can be impacted

54
Q

Danielle NIR out of what range

A

Always check the calibration range

55
Q

20/20/20vision rule

A

Use the 20-20-20 rule. Every 20 minutes, take a 20-second break and focus your eyes on something at least 20 feet away.

56
Q

— g of tolerance , how much for weight cakes

A

0.3 g 1%

Of how much

57
Q

Special detail Shannon taught you about the NIR

A

Put the sample as soon as you get to the area

58
Q

It its an old tanker lot if wont bring

A

A COA

59
Q

What is the bill of lading?

A

Check MFG and disctributor adress this is used to determined reduced or full testing

Make sure its legible

60
Q

Chain of custody bill meeting

A

Always check in and out

61
Q

crude vs next generation

A

crude is like with impurities

next genertaion

62
Q

When doing the balances don’t write the —-!!

A

Units. It’s usually included.

63
Q

Appearance EC

A

Fill in the circles, if it tells you to write it, you should always choose white or white off not both.

64
Q

What would be a considered as metallic particle

A

Anything silver or shiny.

65
Q

Just remember tepentadol gets

A

CE

66
Q

The two big balances are called —

A

Pan

67
Q

How do i know the tolerances for each balances ? What about the weight set?

A

SOP fot the olerances. The actual weights change when the weight set changes.

68
Q

raman sample holders

A

vial holder nose cone (this is used directly against the sample container)

69
Q

according to game stress before cleanup reduces

A

downtime

70
Q

fLOD procedure

A

fLOD Halogen moisture Balance training EC 11-28-16
remember on/off button, tare button, open/close button (last 24 hours, this calibration has no print out )

method button to choose the material or product hit enter

code button to enter sample info

c1 sample a-z letter to switch to alphabet up down arrow c2 batch c3 extra info keep hitting code until I come to the home screen

print out and compare to table
add sample spread it

hit start
wet wight is my weight

71
Q

nATA stans for

A

nxt generation anhydrous thebaine alkaloid

72
Q

when writing a bought mfg chemical write

A

MFG, lot no

73
Q

Mental conflation. Non routines va non controlled

A

It is obvious

74
Q

when to accept non routine samples?

A

SA, PR # or a CoC

75
Q

Noncoformqnces types

A

Events

Deviations

Events -(ICMS)

76
Q

Bill meeting When an auditor comes to check all documents what is this called

A

Audit trail

77
Q

dad detector

A

diode array detector

The main reason for this is that a DAD/PDA can always be set to scan a range of all probable wavelengths, but a single (or multi-wavelength) detector can not.

78
Q

Phone interview

A

Exited introductions meting new people

79
Q

Mobile phase filters

A

0.45 micron MP

80
Q

remmebr to fill forrest zach

A

departmetns –> wilimgnton –> enviromental –>wast inventory

departmetns –> wilimgnton –> hazard communication–> sds

81
Q

Retain Shannon mistake weighing

A

Always make sure it is in the right decimal place.

82
Q

finished product is the only one with —- retain date eveything else that goes on the —- gets 1

A

finished gets 6 year, eveything else in the green lid jar gets 1 year

83
Q

ICMS

A

Instrument calibration maintenance system

Instrument Calibration & Maintenance System (ICMS) is a convenient way to maintain all your records on the equipment, machinery, instrumentation, and very much all of your company assets. Supplied as a separate product or as an integrated part of any Matrix Gemini modules, it holds and reports on any important information. ICMS tracks all your assets, starting from installation, maintenance, repairs, calibration until the disposal of any unusable assets.

84
Q

How to turn off vacuum LOD

A

Turn off punk first then the valve the release the pressure

85
Q

Where are the frops planted ? And what are they called

A

Tazmania poppy seeds

86
Q

DOT

A

Department of transportation

87
Q

Remind yourself of the button to change units in the balances and digits on the pH

A

-

88
Q

Choose what when choosing NIR results

A

Measurement done:

89
Q

Excel keep paswrod

A

For passweod

90
Q

watch for the double negative in the

A

NAOH tanker

91
Q

Product flow chart

A

RM->Wet ->Dry->Mill?->Finishing?

92
Q

Spec says <0.10%

Your results are 0.0045% how should you report it

A

0.005% always report something

93
Q

What’s the difference between an analyst and good analyst ?

A

Analyst produces results and a good analyst ask if it makes sense

94
Q

Post it notes 3 bill

A

Do I understand what they’re asking ?

Do I owe it?

Do I agree?

95
Q

Read well. What about the sample?

A

Is it dried or wet

philip (20 decks)

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