CE

Question 1

CE What is it used for?

Answer 1

Rx Sample

Question 2

CE What is the impurity?

Answer 2

T-3003

Question 3

CE volage

Answer 3

30k watts

Question 4

CE lamp calibration is done how often, how is it done?

Answer 4

Monthly, .Page 13 Agilent lab advisor connect (right upper side), services and diagnostics, DAD, detector test (holmium, intensity) DO ONE AT A TIME, start run, print results write it up in logbook

Question 5

CE sample diluent ACN prep

Answer 5

Molecular sieves, sit for 1-day lasts a month, filter with 0.45 mm into NIR vial, 320g per 4L of acn

Question 6

CE lamp details hwo to turn on

Answer 6

Needs 30 min to equilibrate, control panel, launch (online)

Question 7

CE SOP IOP number

Answer 7

DS-SOP-11311 page 5 vials

Question 8

CE NaOH concentration details

Answer 8

Rxn method 0.1N, preconditioning 1N

Question 9

CE 3 methods type

Answer 9

Preconditioning, rxn method, shutdown

Question 10

CE it is a __________ system

Answer 10

Pressure we need a specific volume, full 600 ml , 300 ml we use the 20-300 ml micropipette

Question 11

CE BE SLN is use to measure the

Answer 11

Background

Question 12

CE method is the ____, sequence is the ___

Answer 12

How, what

Question 13

CE how to run the preconditioning

Answer 13

Run control, sample info, empty vial location

Question 14

CE TIP when you change your method you will know because

Answer 14

It will change your run time

Question 15

CE run test injection

Answer 15

1- change method 
2- run control
3-sample info 
4- vial 2 
5- sample name: SLN - # 
6-fill comment, run method

Question 16

CE review sequence method buttons

Answer 16

-

Question 17

CE sequence up tab

Answer 17

Save sequence template as,

Sequence table to show table

Question 18

CE run control, how to run sequence

Answer 18

Run sequence make sure everything (method, sequence) is good

Question 19

CE how to lock

Answer 19

Up tab user lock session - non privately

Question 20

CE Zach training remember that before applying anything to the chromes you need to select all what was his mistake

Answer 20

Don’t hit overlay select just to the left of that

Question 21

CE how to take out the capillary cartridge

Answer 21

Tilt to the front until you hear a click take it out.

To put another one don’t click it back leave it tilted. Remember to adjust the right side of the capillary with your pinkie.

Question 22

CE Remember to u—d —ls before turning off

Answer 22

Unload vials

Question 23

CE peak tailing should always be

Answer 23

.6 if it’s not that it might indicate a problem

Question 24

CE how to put the injections through a report

Answer 24

• you have to highlight every injection before going to the report tab
• report templates
• there are two reports
• print both