General Lab Stuff Flashcards
When prepping solutions pay attention to all that you add why?
Expiration date
Dryers all dries except are on
Except the 5 are on the east side
gabe uplc wash station where is it
-
CPH
codeine phospahte
You keep doing it! Exp date
7/2017 6/2018 instruments
Whole exp for reagents
Michelle eye contact empower
Look at bottom for processing method
When prepping standards remember to write what down Cristina
And to always look at the
Standard number E number and NQS nnumebr
COA
you may find what about the reactors inside the sample
the lining
Receiving chemicals EC procedure
- intelletrack __receive__ location chemical intentory __ scan sample__ write exp date in the batch
- check binder for COA___ if not google and highlight exp and batch number___ D/I
- scan it __put it in L drive: - swedes – department shared
– quality services – chemical CofAs
You find the scan in applications helpful links Xerox swedes
Justin expression snug is
Great
Michelle Steve npma la training how to find KF values for old batches in SAP
QE13 or QA13, delete inspection points
Mark all the checks on the left, put 1/1/16 on created and enter batch number in the bottom.
Use the new inspection number to search for the info .
nPOB2 fro sg becomes —— npob2 becomes
POBSG ——- nOXY wet, nOXY dry now it follows the same as
NR samples don’t get
SAP
When DEA is reported in SAP remember to write it down in
The logbook
When receiving into intellitrack always check if the material is non controlled or controlled.
All non controlled are immediately disposed of.
Michelle mistake reprocessing
All peaks have to be labeled in impurities run
for expirations dates of MPs and diluents see
Test procedures
OMH
Oxymorphone hydrochloride
Zach palladium in ML are —– with what
deactivated with sodium bisulfite
What to take with you when throwing waste out
Key secondary container mask start accumulation date labels
There is also a container for needles ?
to determine w standard conc
multiply the conc from the sol or stock by the DF
agilent vs waters system that draws sampole
metering piston sample syringe
expiration date from opened for pH buffers
30 days
how are products classified according to mill passes
fine x fine and micronized
Remember COP what (you get asked this a lot)
Location building or whatever
if you circled yes for indefinitely stable
make sure to finishing filling th e sicker when it is opened
HBT
Hydrocodone bitartrate
terms to remeber gabe uplc
needle wash syringe, sample loop, sample manager, low needle, sample prsh
AMA
Morphine base
nPOB reaction train
nPOB 2 wet splits into nPOB2 for POB for sg and nPOB-2
When logging in swabs first do
IT first comments go description
Then sit in your office and do SAP
ACA
anhydrous codeine alkaloid
SIL
Sample in lab
tapentadol train reaction
T2955 T3014 T3028 Wet T3028 Dry
Dilution factor= ?
= solute/total colume
10/50 = 0.2
What is the bill of lading?
Check MFG and disctributor adress this is used to determined reduced or full testing
Make sure its legible
remember how to access
MSDS hazardous waste spreadsheet
According to gabe, A and B mobile pahses are usually what
A aqueous
B is organic
what direction to loosen helium tanks
down
POB 3 wet reaction train
POB 3 wet -> POB 3 dry ->OXY 3 wet -> Oxy3 dry -> splits into oxy3 course oxy 3 first mill pass and oxy 3 STD
ss suit is good until the time of the
last injection
NPMa Steve second shift assay prep
Use the Tare button to get an idea
the weight of the weigh boats can vary
Go as low as possible for assay and as high as possible for impurities
oxy train reaction
CPS thebaine -> nCOB -> splits into POB3 wet and nPOB
AMP and Tap DEA detail
they have separate DEA sample preparation procedure
remember the zach UPLC technique he was teaching jakie
reset SM or whatever
Remember Brett change procedure column
Clips in the union
Circle around to the magnet
Documents to check when receing tankers and what to check on them
-COA
-BO Lading
-Wash Certificate must be signed (Sometimes it ifs dedicated it might not come with it)(sodium hydroxide with letter
Check that they are initial and date and batch from someone from the warehouse
If your NIR residuals are out what to do?
Go to your primary method.
what is a destruction form ?
it destroys a current analytical worksheet and replaces it with another one
Coa STD
Purity factor
Dried?
Ref std/Enumbrr
Retest date
when writing up Working standards in the SLN log book do not forget to
write the conc and the units
freezer safe password
11*1111#
how to fix the pan balances rachel leveling
unlock the hooks in the back turn the wheels in the front
Before acquiring gross weights remember what about the stickers
add all stickers because they add weight
COP that require swabs first need to be —- before going —-
Reviewed swabbing
oxy 3 first mill pass splits into
oxy 3 fine, x fine and micronized
Did I turn it off? I’m so stupid
GC Michhelle
Do not forget the timer when doing
LOD
Start using more —- mistake Christina HCB
Timer
When being the first in the lab
Remember to do the balances and check the 5s thing
OMH final retains go in
The fridge
Methanol / water bubbles
Stir really good
dont forget new tricks NP SAP
deselect all, new selection
transcation to look up older results in SAP
QA13
hit the thing to the side enter batch use that inspection number
how to look up who did something in SAP jaitin sarak
select do the calendar thing and look up in browse JJEDS employee green
empower names for the things you do to the side
transaction codes we use QE51N
what do you do in special cases when fro exam[ple SAP ask you for a certain number of digits and it fails a sample?
you force close it in SAP
SAP <0.05 mistake fix
jatin look to the right the arrow menu
Communication category clean out swabs
Clean out swabs and tucker communication
End of month cycle category
Ph frita vwds
OMH Finals uv vis Jatin kool aid man
Uv VI’s you hit ok instead of finish
Gave fridge tucker 9 things you will explain that to me right? Location of Nishma
Temperature mapping of chart recorder
On the LC 1200 at the end of the month the 2 things that get changed are
The Frits and the column guard
Mentally review column guard and grit change
–tucker
VWD test
Get water Take out column Put in straight line Open purge 5 for 5 min Close 1.5 flow Lamp test
Swab details volume of what
25 mililitros of 1.5 phosphoric
1 dry one wet
Don’t forget the ammonium hydroxide
Always remembering what when doing anything in the works sheet
Always signed a performed by
If you want the oven temp to go lower
Leave the open door
If you want to reduce the chance of something being out of the oven affecting you
Put it ina. Dessiqctr
When trouble shooting impurities in mobile phase remember to
Filter
GC Change syringe don’t forget the
Flap
Get into the habit of writing the exp date last why?
Wait until you add everything the last thing on there is your exp date
How to make your retains faster?
- after your done immediately go to the IT balance to confirm final weight
- ## don’t double check net weight calculation IT will do it for you
