separation techniques Flashcards
mobile phase
a gas or liquid where the molecules are able to move
stationary phase
a solid or thick liquid where the molecules are unable to move
solute
a substance dissolved in a solvent to make a solution
solvent
a liquid in which a solute can be dissolved
solution
a mixture mad up of one substance dissolved in another
why should you use pencil in chromatography?
it is insoluble and won’t dissolve in the solvent and affect the results
filtration
used to separate an insoluble solid from a liquid
chromatography
used to separate the substances in a mixture based on how the components interact with a mobile and stationary phase
what is crystallisation?
the formation of solid crystals as water evaporates from a solution
insoluble
the solid can’t be dissolved in the liquid
crystallisation process
- pour solution into an evaporating dish and gently heat
- once some of the solvent has evaporated or you see crystals start to form, remove the dish from the heat and leave it solution to cool
- salt should start to form crystals as it becomes insoluble
- filter the crystals out of the solutions and leave them in a warm place to dry
evaporation process
- pour the solution into an evaporating dish
- slowly heat the solution
- keep heating until all you have left are dry crystals
when do you have to use crystallisation?
if the salt decomposes when its heated
simple distillation
used for separating a liquid from a solution
simple distillation process
- solution is heated, lowest boiling point evaporates first
- vapour is then cooled, condenses and is collected
- rest of the solution left behind in the flask
issue with simple distillation
can only separate things with very different boiling points as if the temp goes higher than the boiling point of the highest substance, they will mix again
fractional distillation process
- heat the mixture
- the liquid with the lowest boiling point will evaporate first, it will reach the top of the column
- liquids with higher boiling points might also start to evaporate but the column is cooler at the top so they will condense and run back down
- when the first liquid has been collected, you raise the temperature for the next one
filtration process
- filter paper placed in funnel over beaker/flask
- pour mixture through funnel
- insoluble product left on filter paper
what method should be used to separate a soluble solid from a solution if it decomposes when heated?
crystallisation
soluble
can be dissolved
insoluble
can’t be dissolved