separation techniques Flashcards

1
Q

name the 6 physical methods of separation techniques

A
filtration 
evaporation to dryness 
crystallisation
simple distillation 
fractional distillation 
chromatography
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2
Q

define soluble

A

able to dissolve in water

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3
Q

define insoluble

A

not able to dissolve in water

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4
Q

what is suspension

A

it is a liquid-solid mixture

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5
Q

another term of solvent

A

liquid

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6
Q

what does the filtration technique separate

A

separates insoluble solid from liquid in a liquid-solid mixture

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7
Q

what are residues in a filtration technique

A

they are insoluble solids

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8
Q

what is the use of filter paper in a filtration technique

A

to trap residues and allow small substances to pass through

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9
Q

what does the evaporation to dryness technique separate

A

separates dissolved solids in a solid-liquid mixture

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10
Q

what is left behind in the evaporating dish after heating the solution in evaporation to dryness technique

A

residues are left behind

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11
Q

why are the residue is left behind in the evaporating dish in the evaporation to dryness technique

A

that is because it does not decompose on strong heating

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12
Q

what does the crystallisation technique separate

A

separate solid from a solution

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13
Q

describe the steps of crystallisation

A

1) when heating, the solution forms a saturated solution (very concentrated)
2) let it cool, pure crystals will appear
3) filter to obtain the crystals
4) wash crystals with cold distilled water then dry between filter papers

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14
Q

what happens to the solids that are soluble in liquid upon heating in a crystallisation technique

A

solids that are soluble in liquid decompose on strong heating

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15
Q

why wash crystals in cold distilled water in a crystallisation technique

A

to remove impurities

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16
Q

what does it mean to decompose in a crystallisation technique

A

breaks down into sugar only

decompose sugar is carbon+water

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17
Q

define miscible

A

liquids that can mix together

for eg ethanol+water

18
Q

define immiscible

A

liquids that cannot mix together

for eg oil+water

19
Q

what does the simple distillation technique separate

A

separate pure liquid from a solid-liquid mixture? liquid-liquid mixture

20
Q

what does a thermometer used for in a simple distillation

A

to measure the temperature of hot vapour entering the condenser

21
Q

how to know if the liquid in the colonial flask is pure in a simple distillation technique

A

if the thermometer reading remain 100-degree celsius throughout

22
Q

what is the use of boiling chips in a simple distillation technique

A

ensure smooth and even boiling

23
Q

why is a round bottom flask used in a simple distillation technique

A

ensure even heating of the solution

24
Q

what is the use of a condenser in a simple distillation technique

A

provides a cool environment for vapour to condense to water

25
Q

why does the volume of distillate collected reduce in a simple distillation technique

A

this is because some of the hot vapour will escape the condenser instead of condensing it into the beaker

26
Q

why does the ´water in´ in the condenser against gravity in a simple distillation technique

A

as it is efficient in condensing the water vapour and

the water stays longer in the condenser as it is against gravity

27
Q

what does the fractional distillation technique separate

A

separate liquid in a solution

28
Q

what is the use of glass beads in a fractional column in a fractional distillation technique

A

provides large surface area so that vapour can undergo repeated condensation and boiling

29
Q

which liquid will distil first?

the highest or lowest boiling point

A

lowest boiling point

30
Q

why is the condenser sloping downwards

A

to make sure that the pure solvent can run into the beaker

31
Q

explain how the fractional column works

A

vaporization occurs first
the LBP rise up into consider and condenses into liquid and collect as distillate
while LBP is collected, condensation occurs
water vapour of HBP condenses and drops back into the flask
after LBP is collected, temperature rises rapidly

32
Q

difference between fractional and simple distillation

A

1) fractional uses fractional column but simple does not

2) fractional separates miscible liquids but simple separates solvent from a solution

33
Q

what does the chromatography technique separate

A

separate small amount of subs from mixture based on different solubilities of components

34
Q

why is the line drawn by pencil and not pen in a chromatography technique

A

this is because the pencil is insoluble in the solvent and won’t affect the experiment/ interfere with the result

35
Q

why is the starting line above solvent in a chromatography technique

A

to prevent dyes to dissolve into the solvent before the start of the chromatogram

36
Q

what does it say when a dye moves the furthest

A

it is more soluble in the solvent

37
Q

why are the spots far apart on the line

A

to prevent interference with each other

so as to avoid smudging and overlapping dyes

38
Q

what does it say when there is no dye on a chromatogram paper

A

that it does not dissolve in the solvent

aka it is insoluble

39
Q

what does it say when there is one spot on a chromatogram paper

A

it means that the substance is pure

40
Q

how does the solvent separate the components in the sample

A

the solvent dissolves the component

the more soluble the component is, the further it travels