Laboratory Separations Flashcards
Separation Process
a process that separates a mixture into its components based on differences in their properties
Distillation
separates the components based on differences in boiling points
- liquid mixture (solution) is heated until a boiling point of one material is reached
- pure gas removed travels through a condenser and condenses into liquid form, drips into a separate container.
Distillate
Purified liquid from a distillation process
Fractional Distillation
can be used to separate component of a mixture with similar boiling points
- the component with the lowest boiling point evaporates first and is collected after condensing
- sample is collected before the next component condenses
Crystallization
the process by which solid crystals are formed from a homogeneous solution
- crystals can be separated by vaporizing the solvent
- crystals can form a supersaturated solution. as the supersaturated solution cools, the solubility of the solute decreases
- after adding a seed crystal, the solute crystallizes
Seed Crystal
a small or single crystal that is a starting surface for a larger crystal to grow
The solubility of a solute can be decreased by _____ and ____
initiating a chemical reaction; changing the pH of the solution
Absorption
when matter takes in another substance
-spread throughout and becomes part of the structure
Adsorption
when a substance clings to the surface of a solid or a liquid
- does NOT enter the solid or liquid
- creates a film on the surface of the material being clung onto
Adsorbate
the adsorbed substance
Adsorbent
the substance offering a place for the adsorbate to cling
Solvent extraction
a process of removing a component from a mixture by adding a solvent
- utilizes the differences between the solubility of components in the mixture
- component you are trying to take away should dissolve in the added solvent
Chromatography
a group of separation processes used to separate and analyze complex mixtures based on the differences in their structure or composition
-often used in forensic science
Stationary Phase
stationary material in chromatography
Mobile Phase
the mixture that flows over the stationary material in chromatography