Core Practical 5 Flashcards
What is the first step in the oxidation of ethanol to ethanal?
Add acidified potassium dichromate to a pear shaped flask +anti-bumping granules
What is the point in adding anti-bumping granules?
prevent the formation of large gas bubbles that cause violent boiling
(smoother boiling)
What are the colour changes for the reflux and the distillation of acidified dichromate and ethanol?
[For both reactions, the colour change occurs from orange (Cr2O72−) to green (Cr3+).]
Why is heating under reflux used?
Prevents volatile reactants/products from escaping
Ensures even heating
What type of heater do you use for reflux?
An electrical one/ water bath as naked flames can ignite the compounds