C8 - Chemical Analysis Flashcards
What is the set up for a flame test
Platinum or nichrome wire cleaned with concentrated hydrochloric acid - then wire dipped into a sample of the compound - the placed in blue Bunsen flame
Type of metal for the wire for a flame test
Platinum
What type of flame is wire put into for flame tests
Blue Bunsen flame
What colour does lithium go and why
Lithium crimson - both have an I in them
What colour does sodium go and why
Yellow - soooo yellow
What colour does copper go flame test
Green - as 2 ps in copper and 2 es in green
What colour does potassium go?
Lilac - the fourth letter of both is A
What colour does calcium go in flame test?
orange Red
Calcium = Rad = Red
Give 2 possible issues with the flame test
If wire not clean/mixture of metal ions present
Yellow Bunsen burner flame could mask the colour of the flame produced
What is the result of the sodium hydroxide precipitate test for aluminium, calcium and magnesium (colour)
White
Which compound dissolved as well as turning white in the sodium hydroxide precipitate test?
Aluminium
What colour does copper 2 turn in the sodium hydroxide precipitate test
Blue (as they rhyme)
What colour does iron 2 turn in the sodium hydroxide precipitate test?
Green - as II => ee
What colour does iron 3 turn in sodium hydroxide precipitate test
Brown
Iron has o n and brown has own
What 3 compounds are usually used with the sodium hydroxide test? And why?
Copper, iron II, iron III as it has differentiating colours
How do you test the difference between aluminium, calcium or magnesium
Add excess sodium hydroxide solution
Aluminium precipitate dissolves forming a colourless solution
What is necessary to add for a carbonate test?
Hydrochloric acid
How do you conduct the carbonate test
Collect bubbles with a pipette and bubble this into limewater - check if limewater turns cloudy
What is necessary for the sulfate test to be conducted
Add dilute HCl and Barium chloride solution
What forms if sulfate ions are present?
White precipitate
What is necessary for the halide test?
Nitric acid and silver nitrate solution
Give 3 types of precipitate possible for the halide test
White
Cream
Yellow
What is the positive result for chloride in a halide test
Forms white precipitate - as chloride is clean white
What colour does bromide go in a halide ion test
Cream - as A B C
What is the positive colour for iodide
Yellow - I love Yellow
What is an accurate way to test for ions
Flame emission spectroscopy
Give 4 advantages of flame emission spectroscopy
Can identify ions in a mixture
More sensitive
More accurate
More rapid