Topic 8 - Chemical analysis Flashcards
What does pure substance mean?
Something which contained only 1 compound or element throughout it.
How do we test if a substance is pure?
- Measure the substances boiling/melting point
- Compare it to a known pure substance
- The closer your measured value to the actual melting/boiling point, the purer substance is
What do impurities in a substance do to it’s melting/boiling point?
- Impurities in the sample lower the melting point, and increase the melting range
- It will also increase the boiling point and may result in the substance boiling at a range of temps.
What are formulations?
Useful mixtures with a precise purpose, which are made by following a formula. Each component of the formulation contributes so that the formulation meets its required function
What industry are formulations often used in?
The pharmaceutical industry.
What are the 2 phases in chromatography?
- Mobile phase - where the molecules can move
- Stationary phase - where the molecules can’t move.
How do we calculate the Rf value?
Distance travelled by substance/distance travelled by solvent
What is the test for chlorine?
Chlorine bleached damp litmus paper, turning it white.
What is the test for oxygen?
Put a glowing splint inside a test tube containing oxygen, the oxygen will relight the glowing splint.
What is the test for carbon dioxide?
Bubbling CO2 through a solution if calcium hydroxide(limewater)causes it to turn cloudy.
What is the test for hydrogen?
Hold a lit splint at the end of a test tube containing hydrogen, a squeaky pop sound is made.
How do we test for carbonates?
- Add dilute acid into test tube with sample in
- Connect test tube to a test tube with limewater in.
- If carbonates are present, CO2 will be released from the sample and turn the limewater cloudy.
How do we test for sulfates?
1.add drops of HCl, followed by drips if barium chloride solution to a test tube containing the sample.
2. If sulfate ions are present, a white precipitate if barium sulfate will form.
How do we test for halide ions?
- Add some drops of dilute nitric acid followed by silver nitrate solution to the sample.
- Different precipitates will form depending on the halide present
What colour precipitate does chloride give?
White precipitate if silver chloride