Topic 10 - Analysis Flashcards

1
Q

what are flame tests used for?

A

You can carry out a flame test to test for metal ions within compounds.

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2
Q

how are flame tests carried out

A
  • clean a nichrome wire loop by dipping in hydrochloric acid and rinsing with distilled water
  • dip the loop into the sample you want to test
  • put it in the clear blue part of the flame
  • record colour of flame
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3
Q

potassium flame test colour

A

lilac

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4
Q

cooper flame test colour

A

green

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5
Q

sodium flame test colour

A

yellow

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6
Q

lithium flame test colour

A

crimson - red

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7
Q

calcium flame test colour

A

orange - red

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8
Q

Precipitation reaction

A
  • the metal hydroxide formed is insoluble and precipitates out of solution when formed
  • add Sodium Hydroxide to solution of metal ions and note down the colour of precipitate
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9
Q

calcium precipitate

A

white

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10
Q

copper precipitate

A

blue

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11
Q

iron ( Fe2+) precipitate

A

green

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12
Q

iron ( Fe3+ ) precipitate

A

brown

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13
Q

aluminium precipitate

A

white , redissolves in excess NaOH to become colourless

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14
Q

Ammonium ions test (NH4+)

A
  • hold a piece of damp, red litmus paper over ammonia gas
  • if the gas is ammonia, it will turn blue
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15
Q

testing for Carbonate ions

A
  • if you add acid to a carbonate it should react to produce carbon dioxide gas as one of its products
  • bubble the gas produced through limewater
  • if the limewater turns cloudy it is a carbonate
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16
Q

testing for Halide ions

A
  • add dilute nitric acid to get rid of any carbonate impurities
  • add silver nitrate solution
  • it should form a precipitate in solution
17
Q

chloride precipitate

A

white

18
Q

bromide precipitate

A

cream

19
Q

iodide precipitate

A

yellow

20
Q

testing for sulfate ions

A
  • add dilute hydrochloric acid to get rid of any carbonate impurities
  • add barium chloride to it.
  • it should produce a white precipitate of barium sulfate
21
Q

what is Flame photometry?

A

An instrumental method that allows you to identify metal ions by viewing the light the ions emit through a spectroscope

22
Q

About the spectroscope

A

each ion produces a unique line spectrum on the spectroscope, and if there are two or more ions, it shows the line spectrums for all the ions

23
Q

why is flame photometry more useful than flame tests?

A

it can be used to identify more than 1 ion in a mixture, whereas flame tests only work for substances that contain a single metal ion

24
Q

advantages of using machines

A
  • very sensitive
  • very fast
  • can be automated
  • very accurate
  • no room for human error