thermal analysis Flashcards

1
Q

thermogravimetric analysis

A

thermoanalytic technique in which phy and chem properties of materials are measured as a func of increasing temp

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2
Q

TGA thermogram

A

plot of mass against temperature which gives qual and quant info abt substance under study

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3
Q

applications of TGA

A

1) chemical stability above an elevated temp
2) identification and purity det
3) decomposition mechanism
4) det of compsn of alloys and metals
5) amount of filler in a polymeric sample

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4
Q

Limitations of TGA

A

1) limited to study of physical, chemical changes that can be followed by mass change
2) cannot be used for the study of fusion, crystalline transitions, glass transition and crystalline temp, solid state reactions with no volatile products

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5
Q

Differential thermal analysis

A

thermoanalytic technique that can be used as a finger print for identification of materials

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6
Q

DTA thermogram

A

plot of delta T= Ts-Tr versus the reference temp Tr

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7
Q

Applications of DTA

A

1) identification
2) environmental studies
3) quality control
4) purity
5) generation of phase diagram and study of phase transitions

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