Synthesis Flashcards
Dissolving
Aids the reaction by increasing collisions
Filtration
This separates the insoluble solids from liquids to remove the product from the mixture
Crystallisation
This forms crystals from a solution by removing the solvent
Evaporation
This forms a powder from a solution by removing the solvent
Drying
In an oven or desiccator
Removes water left in the product
What are the stages of synthesis
- Deciding which chemicals to use
- Risk assessment
- Mass needed to make a certain mass of product to limit waste
- Select equipment conditions and concentration
- Make product
- Purify product
- Measure the purity by titration to ensure it is suitable for use
Metal + acid
Salt + hydrogen
Acid + metal oxide
Salt + water
Acid + metal hydroxide
Salt + water
Metal Carbonate + acid
Salt + water + co2
Stages of titration
- Add acid to burette and record initial volume
- Measure alkali in volumetric pipette using a pipette filler, add to conical flask
- Add a few drops of indicator
- Slowly add acid to flask until colour change
- Record final volume
To make a titration more accurate
Flask on white tile
Repeat until you get consistent results
Swirl the flask as acid is added
Add acid drop by drop