Separating Techniques - Topic 1 Flashcards

1
Q

What is filtration used to separate?

A

An insoluble solid and a liquid.

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2
Q

Draw a labelled diagram of filtration

A
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3
Q

What is crystallisation used to separate?

A

A soluble solid and a solvent (collects solid).

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4
Q

What technique would you use to separate salt from a solution of salt water?

A

Crystallisation

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5
Q

In crystallisation you heat the solution until it becomes saturated, what does saturated mean?

A

No more of the solute (the thing that dissolves in the solvent) can dissolve

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6
Q

Once you have formed crystals in crystallisation, to obtain dry crystals you filter them and then place them in what?

A

A warming or drying oven

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7
Q

Describe the separating technique of crystallisation.

A

· Heat a solution gently until it becomes a saturated (when no more solute can dissolve) solution.
· Crystals will start to form.
· As the solution cools, the solubility of the solute decreases so more crystals form.
· Filter the crystals. · Dry them in a warming oven.

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8
Q

What is simple distillation used to separate?

A

It separates a solute from a solution. The solute must have a much lower boiling point than the solvent

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9
Q

Describe simple distillation.

A

· The solvent boils.
· The vapours pas through a condenser and condense.
· The pure solvent is collected.

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10
Q

What mixtures are separated by fractional distillation?

A

Two or more liquids that have similar boiling points.

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11
Q

Two or more liquids that have similar boiling points.

A

Substances with different solubilities e.g. different colours of ink or dye.

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12
Q

What is the mobile phase in chromatography

A

The solvent (that travels up the paper).

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13
Q

What is the stationary phase in chromatography

A

The paper

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14
Q

Why should the start line be drawn in pencil?

A

Because pencil will not dissolve and affect the results

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15
Q

Why should the start line sit above the solvent?

A

So that the dots of ink or dye do not wash off the paper.

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16
Q

How is the Rf value calculated?

A

Rf = distance by dye / distance by solvent

17
Q

What does a high Rf value tell us?

A

The substance is more soluble and travelled further.

18
Q

What does a low Rf value tell us?

A

The substance is less soluble and travelled less distance.

19
Q

What should the Rf value always be?

A

A number between 0 - 1

20
Q

What solvents are used in chromatography?

A

Water, alcohol, acetone

21
Q

How can chromatography be used to identify an unknown substance?

A

Compare with a known substance.