REQUIRED PRACTICALS P1 Flashcards
Describe a method to make pure, dry crystal of magnesium sulphate from a metal oxide and a dilute acid.
use magnesium oxide and sulphuric acid
add a fixed volume of sulphuric acid to a beaker and gently heat the acid
add magnesium oxide with a spatula and stir using a glass rod
continue adding magnesium oxide until the magnesium oxide is in excess
you should then filter the solution using a filter paper and funnel to remove excess magnesium oxide
heat the solution in an evaporating basin to until you start seeing crystal to form
turn off the heat and leave the solution to dry
pat the crystals dry with filter paper
carrying out a titration
use pipette to transfer 25cm3 of sodium hydroxide solution into a conical flask
add 5 drops of indicator for example phenol Phalen or methyl orange to the sodium hydroxide in the conical flask
place the conical flask on a white tile, so we see a colour change more clearly
fill a burette with sulfuric acid
start adding acid into the conical flask until we see a colour change, do this while swirling the flask
stop swirling flask and adding acid when you see a colour change for phenophalen pink to colourless for methyl orange yellow to red
read volume of acid added from burette
repeat titration several times until you get readings 0.1cm3 of each other
what are the colour changes fro phenophelon
pink to colourless
what is the colour change for methyl orange
yellow to red
explain why the student should use a pipette to measure the dilute sulphuric acid and a burette to measure the sodium hydroxide solution
pipette measures fixed volume but a burette measure variable volume
test for hydrogen
wooden splint squeaky pop in test tube
test for oxy
glowing splint relights in test tube
test for co2
turns limewater cloudy
test for chlorine
turns damp blue litmus paper red
whats filtration used for
separate insoluble solid from aliquid
temp change practical
use a measuring cyclinder to measure 30cm3 of dilute hydrochloric acid
transfer acid into polystyrene cup
use thermometer to measure the temp of the acid
record this on results table
use measuring cylinder to measure 5cm3 of sodium hydroxide solution and we transfer this to polystyrene cup
place plastic lid over cup with thermometer through middle
gently stir solution using thermometer
look at the temp rise when it stops changing, record the highest temperature reached
rinse out polystyrene cup so that we can repeat experiment using 10cm3 of sodium hydroxide solution
carry out experiment several more times and increase volume of sodium hydroxide solution by 5cm3
repeat whole experiment twice
iv of temp prac
volume of sodium hydroxide
dv of temp prac
max temp reached
cv of temp prac
volume of hydrochloric acid
why do you use polystyrene cup
the experiment we are measuring the temp, this means that we want to reduce heat loss, polystyrene cup is a good insulator so this reduces heat loss