Chemical Analysis Paper 2 (Tests) Flashcards
Test and result for chlorine gas
(gas test)
Test: Damp blue litmus paper
Result: Bleaches it white
Test and result for carbon dioxide gas
(gas test)
Test: Bubble through limewater
Result: Turns it cloudy
Test and result for oxygen gas
(gas test)
Test: Glowing splint
Result: Relights it
Test and result for hydrogen gas
(gas test)
Test: Lit splint
Result: Squeaky pop
Test and result for carbonate ions
(anion test)
Test: React with an acid, bubble gas through limewater
Result: produces salt, carbon dioxide and water
Test and result for sulfate ions
(anion test)
Test: nitric acid , add barium nitrate
Result: Forms a white precipitate
Test for halide ions
(anion test)
Test: Remove impurities with nitric acid, add silver nitrate
Result for chloride ions
(halide test)
Result: White precipitate
Result for bromide ions
(halide test)
Result: Cream precipitate
Result for iodide ions
(halide test)
Result: Yellow precipitate
2 tests for metal ions
(cation test)
- Test: Flame test
- Test: Sodium hydroxide test
Result for lithium ions
(flame test)
Result: Crimson flame
Result for calcium ions
(flame test)
Result: Orange/red flame
Result for potassium ions
(flame test)
Result: Lilac flame
Result for copper(II) ions
(flame test)
Result: Green flame
Result for sodium ions
(flame test)
Result: Yellow flame
Result for magnesium ions
(sodium hydroxide test)
Result: White precipitate
Result for calcium ions
(sodium hydroxide test)
Result: White precipitate
Result for aluminium ions
(sodium hydroxide test)
Result: White precipitate, if sodium hydroxide added in excess then colourless solution
Result for iron(II) ions
(sodium hydroxide test)
Result: Green precipitate
Result for iron(III) ions
(sodium hydroxide test)
Result: Brown precipitate
Result for copper(II) ions
(sodium hydroxide test)
Result: Blue precipitate
What is an instrumental method? Why?
- tests carried out using scientific equipment e.g. Flame emission spectroscopy
- sensitive, fast and accurate unlike chemical tests
Flame emission spectroscopy? How?
- sample is placed in a flame
- light given off is passed through a spectroscope
- line spectrum is outputted
- metal ion identified along with its concentration
Advantages to Flame emission spectroscopy?
Can be used on very small substance
Accurate, sensitive and fast
Disadvantages to Flame emission spectroscopy?
- Specialist staff
- Expensive equipment
Difference in mobile and stationary phase?
(chromatography)
- Mobile phase is the solvent, which the solute can move through
- Stationary phase is the paper, which the solute cannot move through