C14 Chemical Analysis Flashcards

1
Q

What do impurities do to the melting and boiling points of a sample?

A

Lower the melting point and raise the boiling point

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2
Q

What is a formulation?

A

Mixtures that contain specific measured quantities of elements/compounds to ensure efficacy in their usage

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3
Q

What are the 2 phases of chromatography?

A

-Mobile- molecules can move
-Stationary- molecules can’t move

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4
Q

How can Rf values be calculated?

A

Distance travelled by the the substance/distance between solvent front and baseline

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5
Q

What conditions can affect the time a substance spends in the mobile phase?

A

The type of solvent used

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6
Q

What is the stationary phase in paper chromatography?

A

The chromatography paper

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7
Q

(chromatography) The longer a substance spends in the _______ phase, the further it moves up the paper

A

Mobile

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8
Q

What is the test and positive result for chlorine?

A

Holding damp litmus paper up to the reaction vessel- bleaches it white

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9
Q

What is the test for hydrogen?

A

Produces a ‘squeaky pop’ when a lit splint is held to it

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10
Q

What is the test for oxygen?

A

Relights a glowing splint

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11
Q

What is the test for carbon dioxide?

A

Turns lime water cloudy when bubbled through it

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12
Q

What is lime water?

A

Calcium carbonate solution

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13
Q

How can a sample be tested for metal ions using a flame?

A

Dip a nichrome wire in hydrochloric acid and hold it in a blue flame in a Bunsen burner. Withdraw it when no colour is produced. Dip into the sample and hold it into the flame to observe the colour.

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14
Q

Why may testing for ions by observing the colour of the flame they produce be unreliable?

A

If the sample contains multiple metal ions, the flame colours of some may be obscured by the others.

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15
Q

What colour flame do lithium ions produce?

A

Red

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16
Q

What colour flame do sodium ions produce?

A

Yellow

17
Q

What colour flame do potassium ions produce?

A

Purple

18
Q

What colour flame do calcium ions produce?

A

Orange-red

19
Q

What colour flame do copper ions produce?

A

Green

20
Q

How can you test for metal ions using hydroxides?

A

Add a few drops of sodium hydroxide solution to the sample you are testing. If a coloured precipitate forms, you can deduce which metal was in the sample.

21
Q

What are the products of a reaction between a carbonate and a dilute acid?

A

A salt, water and carbon dioxide

22
Q

Describe how flame emission spectroscopy works:

A

A sample is placed in a flame, exciting the electrons in the ions. As the electrons drop back to their original energy levels, specific wavelengths of light are released. These pass through a spectroscope which show a line spectrum.

23
Q

What are the advantages of using machines in chemical analysis?

A

-Very sensitive
-Accurate
-Efficient

24
Q

What colour is a calcium hydroxide precipitate?

A

White

25
Q

What colour is a copper (II) hydroxide precipitate?

A

Blue

26
Q

What colour is an iron (II) hydroxide precipitate?

A

Green

27
Q

What colour is an iron (III) hydroxide precipitate?

A

Brown

28
Q

What colour is an aluminium hydroxide precipitate?

A

White, then dissolves to be colourless

29
Q

What colour is a magnesium hydroxide precipitate?

A

White