4.4 Gravimetric Analysis Flashcards
1
Q
gravimetric analysis use
A
determine the mass of an element or compound in a substance
2
Q
used to determine the mass of an element or compound in a substance
A
gravimetric analysis
3
Q
technique of gravimetric analysis
A
- using an accurate balance, including the tare function
- using a weighing boat
- weighing by difference
- weighing accurately approximately
- heating to a constantly mass
4
Q
heating to a constant mass
A
- heating a substance
- allowing to cool in a desiccator to prevent absorption of water
- weighing
- repeating the steps of heating, cooling and weighing until no further changes in mass are observed
5
Q
- heating a substance
- allowing to cool in a desiccator to prevent absorption of water
- weighing
- repeating the steps of heating, cooling and weighing until no further changes in mass are observed
A
heating to a constant mass
6
Q
method of gravimetric analysis
A
- The substance is converted into another substance of known chemical composition, which can be readily isolated and purified
- The conversion can occur either through precipitation or volatilisation
- In precipitation conversion the substance undergoes a precipitation reaction. The precipitate is separated from the filtrate and the filtrate tested to ensure the reaction has gone to completion. The precipitate is washed, dried to constant mass and then weighed
- In volatilisation conversion the substance is heated and any volatile products (often water) are evaporated. The substance is heated to constant mass and the final mass recorded
7
Q
- The substance is converted into another substance of known chemical composition, which can be readily isolated and purified
- The conversion can occur either through precipitation or volatilisation
- In precipitation conversion the substance undergoes a precipitation reaction. The precipitate is separated from the filtrate and the filtrate tested to ensure the reaction has gone to completion. The precipitate is washed, dried to constant mass and then weighed
- In volatilisation conversion the substance is heated and any volatile products (often water) are evaporated. The substance is heated to constant mass and the final mass recorded
A
gravimetric analysis
8
Q
A