required practical 2: measurement of enthalpy change Flashcards
formula for calorimetric enthalpy change (Q)
Q = m X C X ∆t
Q = energy change (J)
m = mass (g)
C = heat capacity
∆t = change in temp
general method of calorimetry (solution and solid)
place polystyrene cup in glass beaker
measure desired volume of solution using volumetric pipette and transfer to cup
place thermometer in cup and measure initial temp
continue to measure temp at regular intervals until temp remains constant
if solid reactant is used - weigh before and after
stir mixture
common errors during calorimetry experiments
heat energy lost to the surrounding
reaction may be incomplete
incomplete combustion - if fuel is used
how can you improve the accuracy of this experiement
use electronic temperature sensor
use a flame calorimeter as less heat is lost
why should glass beakers not be used during this experiment
glass is a poor conductor
how is accuracy of this experiment improved
using insulators or lids to prevent heat loss
how is the data from the method used to determine the temp change
record initial temp
record temp at regular intervals
plot graph - temp x time
extrapolate to point of addition
determine change in temp