MIDTERM GROUP 1 ANIONS Flashcards

1
Q

the calcium salts of the anions Group 1 are ___________ in netural or slightly basic solution.

A

insoluble

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2
Q

Group 1 Anions Precipitating Agent

A

Calcium Acetate

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3
Q

Group 1 Anions are divided into 2 subgroups by the action of _____________

A

dilute Acetic Acid

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4
Q

They are insoluble to 3M HAc

A

Calcium Flouride and Calcium Oxalate

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5
Q

The Soluble groups should be analyzed immediately after solution is ____________

A

effected

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6
Q

FIRST DAY OF ANALYSIS involves the detection of what ion?

A

Carbonate Ion

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7
Q

FIRST DAY OF ANALYSIS: In the first step, what are you going to put inside the test tube (mixture)

A

10 drops of 3M HCl
10 drops of distilled water
0.1g of KClO3

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8
Q

10 drops of 3M HCl
10 drops of distilled water
0.1g of KClO3
Then add 10 drops of unknown sample.

What indicates the presence of Carbonate Ion?

A

Vigorous effervescence (murag sa sparkles sa wine)

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9
Q

FIRST DAY OF ANALYSIS: What amount of distilled water will you put in the remaining unknown sample?

A

equal to the number of drops of the remaining unknown sample

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10
Q

FIRST DAY OF ANALYSIS: Amount of 1.5 M Na2CO3 solution to be added after the water bath for 2 minutes?

A

equal to the number of drops of the sample

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11
Q

FIRST DAY OF ANALYSIS: In the first centrifuge, which part of the separated molecules are you going to discard?

A

precipitate

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12
Q

FIRST DAY OF ANALYSIS: The centrifugate obtained in procedure number 2 what Solution are you going to add to make the precipitation complete?

A

2M Ca(Ac)2 drop by drop

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13
Q

What is the maximum drops for 2M Ca(Ac)2?

A

15 drops

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14
Q

In procedure #3, after the centrifuge, what separated part are you going to discard?

A

centrifugate

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15
Q

The residue may contain?

A

Insoluble:
- calcium salts of carbonate
- sulfite
- arsenite
-arsenate
- phosphate
-oxalate
-flouride ions

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16
Q

What solution are you going to add to the residue/precipitate before the last centrifuge of the Day 1 Analysis?

A

15 drops of 3M HAc