MIDTERM GROUP 1 ANIONS Flashcards
the calcium salts of the anions Group 1 are ___________ in netural or slightly basic solution.
insoluble
Group 1 Anions Precipitating Agent
Calcium Acetate
Group 1 Anions are divided into 2 subgroups by the action of _____________
dilute Acetic Acid
They are insoluble to 3M HAc
Calcium Flouride and Calcium Oxalate
The Soluble groups should be analyzed immediately after solution is ____________
effected
FIRST DAY OF ANALYSIS involves the detection of what ion?
Carbonate Ion
FIRST DAY OF ANALYSIS: In the first step, what are you going to put inside the test tube (mixture)
10 drops of 3M HCl
10 drops of distilled water
0.1g of KClO3
10 drops of 3M HCl
10 drops of distilled water
0.1g of KClO3
Then add 10 drops of unknown sample.
What indicates the presence of Carbonate Ion?
Vigorous effervescence (murag sa sparkles sa wine)
FIRST DAY OF ANALYSIS: What amount of distilled water will you put in the remaining unknown sample?
equal to the number of drops of the remaining unknown sample
FIRST DAY OF ANALYSIS: Amount of 1.5 M Na2CO3 solution to be added after the water bath for 2 minutes?
equal to the number of drops of the sample
FIRST DAY OF ANALYSIS: In the first centrifuge, which part of the separated molecules are you going to discard?
precipitate
FIRST DAY OF ANALYSIS: The centrifugate obtained in procedure number 2 what Solution are you going to add to make the precipitation complete?
2M Ca(Ac)2 drop by drop
What is the maximum drops for 2M Ca(Ac)2?
15 drops
In procedure #3, after the centrifuge, what separated part are you going to discard?
centrifugate
The residue may contain?
Insoluble:
- calcium salts of carbonate
- sulfite
- arsenite
-arsenate
- phosphate
-oxalate
-flouride ions