Chemical Analysis Flashcards

1
Q

What is a pure substance in chemistry

A

A substance is a single element or compound that is not mixed with any other substance

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2
Q

What is a pure substance in everyday language

A

A substance that has had nothing added to it

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3
Q

What is a formulation

A

A mixture that has been designed as a useful product, with carefully measured components so the product has desired and required properties.

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4
Q

What does Paper Chromatography do

A

Separates the different dyes in an ink

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5
Q

Describe paper chromatography method (7 steps)

A

1- take filter paper and draw line in pencil near bottom (base line)
2 - add sample of ink to baseline
3 - Fill beaker with shallow amount of solvent
4 - Place filter paper into solvent
5 - Don’t submerge ink in solvent
6 - Place lid on top of beaker to stop the solvent evaporating
7 - Wait for solvent to seep up paper, dyes will dissolve in solvent and move up with it at different rates
8 - Take paper out and leave to dry

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6
Q

What happens to un soluble substances in paper chromatography

A

Stay on the base line

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7
Q

What is the mobile phase

A

Substance the molecules can move in (solvent)

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8
Q

What is the stationary phase

A

Substance the molecules can’t move in (paper)

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9
Q

Why do more soluble substances move up further

A

Spend more time in the mobile phase, so move faster
Less soluble are more attracted to the paper and spend more time in the stationary phase

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10
Q

How to calculate Rf value

A

Distance travelled by substane / distance travelled by solvent

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11
Q

Test for hydrogen

A
  • Burning splint held at the open end of a test tube of the gas
  • Hydrogen burns rapidly with a pop sound
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12
Q

Test for oxygen

A
  • Glowing splint inserted into a test tube of the gas
  • The splint relights in oxygen
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13
Q

Test for carbon dioxide

A
  • Use aqueous solution of limewater, will turn cloudy when co2 is bubbled through it
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14
Q

Test for chlorine

A
  • Damp litmus paper bleaches and turns white in presence of chlorine gas
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15
Q

What do lithium compounds result in during flame test

A

Crimson flame

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16
Q

What do sodium compounds result in during flame test

A

Yellow flame

17
Q

What do potassium compounds result in during flame test

A

Lilac flame

18
Q

What do calcium compounds result in during flame test

A

Orange/red flame

19
Q

What do copper compounds result in during flame test

A

Green flame

20
Q

What solutions form white precipitate and when

A

When sodium hydroxide solution is added,
Aluminium
Calcium
Magnesium
But magnesium hydroxide precipitate dissolves in excess sodium hydroxide solution

21
Q

When sodium hydroxide is added, what colour precipitate does copper (ii) form

A

Blue

22
Q

When sodium hydroxide is added, what colour precipitate does iron (ii) form

A

Green

23
Q

When sodium hydroxide is added, what colour precipitate does iron(iii) form

A

Brown

24
Q

Test for carbonates

A

Will react with dilute acids to form co2, which can be identified using limewater

25
Q

Test for halides

A

Produces precipitates with silver nitrate, if in the presence of dilute nitric acid

26
Q

What colour precipitate is silver chloride

A

White

27
Q

What colour precipitate is silver bromide

A

Cream

28
Q

What colour precipitate is silver iodide

A

Yellow

29
Q

Test for sulphates

A

Produce a white precipitate with barium chloride solution in the presence of HCL

30
Q

Give an example of an instrumental method of analysing elements and compounds

A

Flame emission spectroscopy

31
Q

Explain briefly how to carry out flame emission spectroscopy

A

Place sample into a flame and the light given out is passed through a spectroscope.
The output is a line spectrum that can be analysed to identify metal ions and their concentration