C10- chemical analysis 🧪 Flashcards

1
Q

What is a pure substances ?

A
  • a pure substance, is a single element or compound not mixed with any other substance
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2
Q

How can a substance be tested, to determine if it is pure ?

A
  • a substance’s melting and boiling point can be measured.
  • this is because, a pure substance will melt at a specific fixed temperature
  • and a pure substance, will have a specific boiling point
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3
Q

How can a substance be tested, to determine if it is impure ?

A
  • like pure substances, a substance’s melting and boiling point can be measured.
  • this is because, impure substances melt and boil over a range of temperatures
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4
Q

[Extra] Why is it important to test for pure and impure substances ?

A
  • For substances used in preparing food and drugs, it is important that only permitted pure substances are being used.
  • this is because, if a substance is impure, and laced with some other substances, these unapproved impurities might not be safe for human consumption- which could lead to undesirable effects on human health.
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5
Q

What is a formulation ?

A
  • a formulation, is a complex mixture that has been designed as a useful product
  • [and in a formulation, the quantity of each component is carefully measured, so that the product has the required properties]
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6
Q

Name some examples of a formulation ?

A
  • fuels
  • paints
  • cleaning products
  • medicines
  • alloys
  • fertilisers
  • and, food
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7
Q

RECAP: What is paper chromatography ?

A
  • paper chromatography, is a physical separation technique that separates substances based on their different solubilities
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8
Q

Describe a method you would do to carry out paper chromatography [5]

Hint: draw, pipette, place, solvent, dry

A
  • draw a pencil line across chromatography paper (about 1 cm above the bottom)
  • use a pipette, or capillary tube, to add small spots of each ink (A,B, C and D) to the line on the paper, as well as unknown ink (U) (equally spread across the paper)
  • place the paper into a container with a suitable solvent (e.g. water) in the bottom - making sure the pencil line is above the water line
  • and allow the solvent to move through the paper, but remove the chromatogram before it reaches the top
  • then allow the chromatogram to dry, and measure the distance travelled by each spot and by the solvent
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9
Q

With chromatography, is there a limit to how many substances we can test?

A
  • no, with chromatography this can be done with several colours; there has to be enough space on the paper.
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10
Q

What is the stationary phase in paper chromotography?

A
  • In paper chromatography, the stationary stage is called the paper- because it doesn’t move.
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11
Q

What is the mobile phase in paper chromatography?

A
  • In paper chromatography, the mobile phase is the solvent- since it does move.
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12
Q

In chromatography, what’s the difference between the stationary 🆚️ mobile phase?

A
  • the stationary stage is called the paper- because it doesn’t move
  • ; the mobile phase is the solvent- since it does move.
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13
Q

In paper chromatography, how do we know if a colour is a single substance?

A
  • there will be only one spot
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14
Q

Why does paper chromatography work? [3]

A
  • paper chromatography works, because each chemical in the mixture will be attracted to the stationary phase (the paper), to a different extent.
  • and chemicals that are strongly attracted to the stationary phase (the paper) will not move very far.
  • chemicals that are weakly attracted, will move further up the paper.
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15
Q

What will a pure chemcial produce, 🆚 chemicals in a mixture?

A
  • a pure chemical produces singles spot in all solvents
  • ; a chemical in a mixture may separate into different spots, based on the solvent.
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16
Q

In paper chromatography, why do we draw our starting line in pencil instead of pen ?

Hint: ⬆️

A
  • We draw our starting line in pencil, since if it was in pen: the pen ink would move up the paper with the solvent.
17
Q

What is the calculation for Rf value ?

A
  • Rf value= distance moved by substance âž— distance moved by solvent
18
Q

What is the test for hydrogen gas ?

A
  • use a burning splint held at the open end, of a test tube of a gas.
  • and if hydrogen gas is present, hydrogen gas burns rapidly with a squeaky pop sound
19
Q

What is the test for oxygen gas ?

A
  • use a glowing splint inserted into a test tube of oxygen gas, and oxygen has will relight a glowing splint
20
Q

What is the test for carbon dioxide gas ?

A
  • use an aqueous solution of limewater [calcium hydroxide], and draw some of the gas into a plastic pipette
  • and when carbon dioxide is shaken with or bubbled through limewater, the limewater turns cloudy
21
Q

What is the test for chlorine gas ?

A
  • insert damp litmus paper, into the mouth of a test tube containing chlorine gas
  • and if chlorine gas is present, the damp litmus paper is bleached and turns white