Analysis Flashcards

1
Q

What would we use the melting point for?

A

To help identify a product and how pure the product is

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2
Q

Why do we need to record the temperature for the start and end of melting?

A

The range indicates how impure the sample is, a large melting range means a product has more impurities

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3
Q

between what range will a pure substance melt within?

A

0.5oC of true melting point

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4
Q

Describe how to make a standard solution from a solid

A
  1. weigh the required mass of solid with weighing boat
  2. pour 100cm^3 of deionised water into a 250cm^3 beaker, transfer the solute and weigh the boat to calculate the exact mass of solute added
  3. Stir the mixture to ensure it fully dissolves
  4. Transfer to a 250cm^3 volumetric flask, adding the washings of the beaker and stirring rod as well.
  5. Fill to within 1cm of the mark on the neck and use a dropping pipette to bring up to 250cm^3 while looking at it at eye level
  6. Place the stopper in and invert it shaking thoroughly to make a homogenous mixture
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