Week 2: Pot distillation, column distillation, maturation in oak and inert vessels Flashcards
What can be used to heat a still other than steam?
Direct heat / open flame
What is the heat requirement for Cognac distillation?
Direct heat (better for Maillard reaction)
What is the first batch created by the first distillation in pot stills called?
Low wine or pot ale
What is the typical abv of the low wine?
25% abv
What are the 3 main condensers?
- Shell
- Coil Worm Tube
- Others (like the rustic design of some mezcal distillers)
What are the main 2 heat sources of stills?
- Direct heat
- Indirect steam heating (coils, jackets, external heat exchangers)
What are the 2 batch products of the first distillation?
- Low wine (25% abv) or pot ale
- Liquid waste (little ethanol and all of the non volatile fractions)
What are the 3 products of the second distillation?
- Heads & Tails
- The heart
- Liquid waste
What are the 3 challenges of pot distillation?
- High operating costs
- Limited rectification results (up to about 80% abv max)
- Group 3 fractions hard to eliminate
What system is used for solid state fermented base material?
Steam injection
What is the aim of the second distillation?
Concentrate and select the wanted fractions
What are the two challenges that distillers have to face when using direct heat?
- Fires are difficult to control precisely.
- It is difficult to maintain an even heat across the base of the pot (risk of scorching).
What is the most widely used method for heating a still?
Indirect steam heating. The steam does not come into direct contact with the liquid it is heating.
Name three ways indirect steam can be used to heat a still?
Coils
Jackets
External heat exchangers.
How is steam introduced in a still that uses steam injection as heat source?
The steam is introduced at high pressure through an inlet at the base of the still.
Name the three key ways reflux can be managed in a pot still?
- Still height
- Controlling the heat input
- Using dephlegmators/head condensers.
What are the three types of condenser used with pot stills?
- Shell and tube
- Worm tub
- ‘Bowl of water’ condensers used in some Mezcal stills.
In batch distillation, what is the aim of the first distillation?
Remove some of the water and the Group 4 fractions from the alcoholic liquid.