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Final Chem > Oxidation Of Cyclohexanol To Cyclohexanone > Flashcards

Oxidation Of Cyclohexanol To Cyclohexanone Flashcards

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1
Q

What are the reactants

A

The reactants are cyclohexanol sodium hypochlorite and acetic acid

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2
Q

What are the products

A

The products are cyclohexanone hydrogen chloride water and sodium acetate

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3
Q

Cyclohexanol precaution

A

Irritation

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4
Q

Cyclohexanone precaution

A

Flammable

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5
Q

Glacial acetic acid precaution

A

Flammable

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6
Q

Why RN a OCL and glacial acetic acid used in the preparation of cyclohexanone

A

They are used because NAOCL is the oxidizing agent and acetic acid is the catalyst

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7
Q

What is the purpose of using NaOCl3

A

The purpose of using it is to neutralize any remaining acetic acid

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8
Q

What is the common name for NAHC03

A

The common name is baking soda

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9
Q

What is the purpose of using NAHS03

A

The purpose is to neutralize any remaining oxidizing agent

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10
Q

What is the common name or NAHS03

A

The common name is sodium bisulfite

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11
Q

Define salting out

A

Salting out is the organic compound is much less soluble in a solution with high ionic strength

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12
Q

Define oxidation

A

Is the increasing number of CO bonds and the decreasing number of CH bonds

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13
Q

Define reduction

A

Is the decreasing number of CO bonds and increasing the number of CH bonds

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14
Q

What physical property is used to separate cyclohexanone from an unreacted cyclohexanol?

A

Density and solubility

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15
Q

Is there an HMNR signal for CO bond in cyclohexanone

A

No there are no signals or the CO bond in cyclohexanone because there are no hydrogen attached to this area

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16
Q

What major pig do you look at for the I R of cyclohexanol

A

The major peak we look for is 0H due to the cyclohexanol being an alcohol the range of an OH is 3200 to 3600

17
Q

For talons test what is a positive test

A

A positive test indicated by silver metal a black or silver precipitation will form

18
Q

DNPH test, what is a positive test

A

A positive test is the presence of precipitation

19
Q

For chronic acid test what is a positive test

A

A positive test is the formation of a blue green precipitate

20
Q

What were the results for the comic acid test

A

The results were all orange to blue green except for 2-methyl-2-butanol which was NR

21
Q

What were the results for the DNPH test

A

There was no reaction or propanol to Metal 2 butanol isopropyl alcohol and 2-propanol.
There was precipitate for cyclohexanone acetophenone, acetone, and pentan-2-one.

Final Chem (8 decks)

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