Laboratory Flashcards
What is a Maximum Residual Disinfectant Level (MRDL)?
Maximum measurement of disinfection allowed in order to prevent disinfection by-products
What is the MRDL for Chlorine, Chloramines, and Ozone?
Chlorine = 4.0 mg/L Chloramines = 4.0 mg/L Ozone = 0.0 mg/L
What is the MRDL for Fluoride?
- 0 mg/L (Primary)
2. 0 mg/L (Secondary)
What is Modeling in relation to fluoride?
Drinking water with too much fluoride causes brown stains on teeth
What is the target fluoride range and optimum level?
Range - 0.6 mg/L - 0.8 mg/L
Optimum - 0.7 mg/L
How often must the water be tested for fluoride?
Once a day at representative sites
How often must samples be sent to the state lab for fluoride analysis?
One sample per month taken from a representative location in the distribution system and submitted to the state laboratory of hygiene. The sample submitted to the state laboratory of hygiene shall be a portion of a split sample so that the operator can determine the fluoride concentration with the operator’s equipment and compare it to the state laboratory results. The fluoride concentration obtained by the operator shall be noted on the data sheet prior to submission to the state laboratory.
Describe the sample container requirements for collecting fluoride samples
Glass/Plastic - State will send you bottle.
Rinse initially with distilled water
then rinse with sample water
What lab test is the chemical DPD used to detect?
DPD = N,N-diethyl-p-phenylenediamine
Chlorine & Chloramines
What lab test is the chemical SPADNS used to detect?
SPADNS = 4,5 Dihydroxyl-3-(p-Sulfophenylazo)-2,7-Naphthalene-Disulfonic Acid Trisodium Salt
Fluoride
What is the specific ion test used for?
calibrate to detect specific ion…. probably need more info this is vague
Describe the free chlorine residual test utilizing the DPD method
Calibrate (Zero Out) Add DPD reagent to bottle(powder) Add sample Shake Test with pocket unit (is this a small spectrophotometer?)
Darker pink = more chlorine
Wavelength will identify Cl2 (530 nm)
Describe the Fluoride procedure test utilizing the SPADNS method
Absorbs fluoride and becomes a LIGHTER shade of red (opposite Cl2)
Compare to known fl- sample using a spectrophotometer.
Fl- = 580 nm
Temp of SPADNS, Temp of Sample, Temp of known sample should all be the same
What is the correct way to read a meniscus?
Concave = Water meniscus Convex = Mercury meniscus
Describe how to run a pH test
First add 7 buffer
Then add either 4 or 10 buffer depending on where you think the pH falls (this is called bracketing)
4 buffer if its between 0-7
10 buffer if its between 7-14