L7/8- Multiphase systems Flashcards

1
Q

Continuous phase

A

Mass transfer more rapid - turbulent diffusion

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2
Q

Disperse phase

A

Proceeds by droplet breakup and recoalescence

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3
Q

When is pH only controlled?

A

When aqueous phase continuous

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4
Q

What is insensitive to agitation?

A

Phase boundaries are insensitive to agitation

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5
Q

How does increasing agitator speed affect continuity?

A

Increasing agitator speed destabilises heavy phase continuity/ stabilises light phase continuity

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6
Q

What are the axis on a phase diagram related to phase continuity?

A

Volume fraction light phase v agitator speed/power

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7
Q

Controlling phase dispersion

A

Add phase to be dispersed to agitated vessel, until volume fraction is required

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8
Q

What phase will be continuous of an agitator is stopped and re-started?

A

Phase agitator sits in will become continuous (this is usually the heavy phase)

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9
Q

What type of liquid is best to have as disperse phase?

A

High viscosity liquid as disperse phase;
Effective mixture viscosity reduced & heat transfer coefficients improved

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10
Q

How to go from heavy continuous to light continuous phase?

A

Add light phase / increase volume fraction
(vice versa)

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11
Q

Effect of baffles & what can happen without?

A

Good dispersion, otherwise surface vortices form and overtopping danger

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12
Q

Agitated vessel; mean specific power consumption, epsilon m

A

epsilon m = P/(V*p)

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13
Q

Critical rotation speed, NJD:

A

If agitator started in heavy phase, there is a critical rotation speed NJD where the light layer above is dispersed in droplets (light in heavy)

(vice versa)

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14
Q

How would a decreased vessel size and heavy-in-light system affect power required?

A

Both would require more work/rotational power

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15
Q

What impeller best used for Solid suspensions?

A

Angled-blade turbine or marine propeller:

Directs flow downward to scour bottom and creates an upward velocity

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16
Q

Dispersion and mass transfer of gases in liquids

A

Mass transfer slow unless gas is well dispersed and agitated
Poor mass transfer if only rise of clouds of small bubbles for some agitation
Type of gas injection device little effect on bubble size distribution

Position of gas injection crutial

17
Q

What turbine is best for gas dispersion?

A

Rushton turbine

18
Q

What is a Rushton turbine?

A

Shedding of bubbles in high shear regions near tip, so small bubbles and high values of kL*a

19
Q

What is a Frings Aerator?

A

Agitator dic creates partial vacuum at axis that sucks gas through sleeve around shaft.

Disperses gas as bubbles

20
Q

Flow number, Fl

A

Fl = [Q]/[(N)*(Da^3)]

21
Q

Critical agitator speed for bubbles to be dispersed and fill reactor above disc:

A

Fl <= 30Fr[(Dt/Da)^(-3.5)]

22
Q

Whole vessel to be full of bubbles (& below agitator)

A

Fl <= 0.2(Fr^0.5)[(Dt/Da)^0.5]