Hardness Flashcards
Maximum sample holding time
28 days, but recommended immediate
What titrant is used for hardness
0.01 M EDTA
What color will the solution turn when fully titrated
magenta to stable blue
What is the multiplication factor used for a volume of 100 mL
10X
Frequency of QC standard for Hardness
Monthly
What volume of sample is used
50 mL
What volume of buffer is used
1.0 mL
How much color indicator is used
3 drops
Volume of calcium added for standardization
20 mL standard to 30 mL DI water
How many replicates are completed for standardization
2 (duplicates)
What volume of titrant is acceptable for the standardization blank
less than 0.1 mL (about 2 drops)
Standardization acceptance criteria
5% nominal (19.0-21.0 mL titrated)
Can a correction factor be applied
no, we use commercially bought EDTA
Expiration of reagents and indicators
1 year after opening, or manufacturers exp date