Hardness Flashcards

1
Q

Maximum sample holding time

A

28 days, but recommended immediate

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2
Q

What titrant is used for hardness

A

0.01 M EDTA

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3
Q

What color will the solution turn when fully titrated

A

magenta to stable blue

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4
Q

What is the multiplication factor used for a volume of 100 mL

A

10X

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5
Q

Frequency of QC standard for Hardness

A

Monthly

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6
Q

What volume of sample is used

A

50 mL

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7
Q

What volume of buffer is used

A

1.0 mL

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8
Q

How much color indicator is used

A

3 drops

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9
Q

Volume of calcium added for standardization

A

20 mL standard to 30 mL DI water

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10
Q

How many replicates are completed for standardization

A

2 (duplicates)

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11
Q

What volume of titrant is acceptable for the standardization blank

A

less than 0.1 mL (about 2 drops)

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12
Q

Standardization acceptance criteria

A

5% nominal (19.0-21.0 mL titrated)

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13
Q

Can a correction factor be applied

A

no, we use commercially bought EDTA

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14
Q

Expiration of reagents and indicators

A

1 year after opening, or manufacturers exp date

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