Exp 9 Flashcards

1
Q

Exp 9:
1. Place __ drops each of the ff aqueous solutions to separate centrifuge tubes: 1M Ba(NO3)2, 1M Mg(NO3)2, 1M Ca(NO3)2, and 1M Sr(NO3)2. Make each solution basic by adding a few drops of _____. Confirm using filter paper

A
  • 20
  • 6M NH4OH
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2
Q

Exp 9:
2. Carefully add 1mL _____, and stir. Put the centrifuge tube into hot (but not boiling) water and leave in the water bath for ___ minutes. Stir occasionally.

A
  • 1M (NH4)2CO3
  • 2
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3
Q

Exp 9:
3. Centrifuge and decant the supernatant liquid into ______

A

another centrifuge tube

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4
Q

Exp 9:
4. To the test tube containing Ba2+, wash the precipitate with ____. Centrifuge out the precipitate and discard the wash

A

2mL water

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5
Q

Exp 9:
5. Add _____ to the precipitate in step 4 and stir to dissolve the remaining solid residues

A

0.5 mL 6M acetic acid

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6
Q

Exp 9:
6. To confirm the presence of Ba2+, add _____ of water and 5 drops of ___ and mix. Then add 0.5 mL _______

A
  • 1 mL
  • 6M NH3
  • 1M K2CrO4
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7
Q

Exp 9:
7. To the remaining test tubes, add ______ until the solution is basic. Stir thoroughly to ensure that the entire sample is basic

A

6M NH3

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8
Q

Exp 9:
8. To confirm the presence of Sr2+, add _________

A

1mL of saturated CaSO4 solution

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9
Q

Exp 9:
9. To confirm the presence of Ca2+, add ______ and mix well

A

0.5 mL 1M K2C2O4

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10
Q

Exp 9:
10. To confirm the presence of Mg2+, add 0.5 mL ________ and mix well. Stir the solution, warm it gently in the hot water bath, and let it stand for a minute

A
  • 1M Na2HPO4
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