chemical analysis - C8 Flashcards
what is a pure substance
a substance that contains only one type of element or compound
what is the difference of the boiling points of pure and impure substances
pure substances boil at specific temperatures
impure substances boil over a range of temperatures
us checking for boiling point a physical or chemical test
physical
what is formulation?
-they are mixtures that have a specific formula
-a mixture made suing precise amounts of different components, each having a specific purpose
give examples of formulations
paint, medicines , cleaning agents, fertilisers, alloys, some food and drinks
what is chemical analysis
the instruments and methods we use to identify, separate and quantify different substances.
what are the precautions to take when testing for chlorine gas
-wear a gas mask
- do it in a fume cupboard
how do we test for carbonate ions?
when a carbonate reacts with an acid it forms a salt, carbon dioxide and water
-so add dilute HCL
-collect any gas and bubble it through lime water
-if it turns cloudy then carbonates were present
how do we test for sulfate ions
-add dilute HCL to get rid of any carbonates
-add barium chloride
-if a white precipitate forms, barium sulfate has formed which means sulfate ions are present
how do we test for halides
-add dilute nitric acids to get rid of any impurities
-then add silver nitrate
-if it forms a white precipitate = chloride ions
-cream precipitate = bromide ions
-yellow precipitate = iodide ions
how can we test for cations
flame tests and sodium hydroxide tests
how do you carry out a flame test
-dip a nichrome wire in some HCL, then rinse it off with water and put it over a bunsen burner flame to clean it
-the dip the nichrome wire loop in the compound you want to test
-put it in the blue part of the flame
what flame do sodium ions give
yellow
what flame do potassium ions give?
lilac
what flame do lithium ions give
crimson
what flame do copper ions give
green
what flame do calcium ions give
orange-red
how do the sodium hydroxide test work
when a metal ion reacts with sodium hydroxide it forms a precipitate which makes the solution a certain colour
what precipitate do copper ions give
blue precipitate
what precipitate do calcium ions give
white
what precipitate do iron 2 ions give
green
what precipitate do iron 3 ions give
brown
what precipitate do magnesium ions give
white
what precipitate do aluminium ions give
white but if excess sodium hydroxide is added it turns colourless
how does flame emission spectroscopy work
-metal ion is heated until it emits light
-the light is detected by a spectroscope which can detect the different wavelengths of light
-each cation produces a unique combination of wavelengths and will put these onto a unique spectrum
-then we can identify the cation
what does the intensity of the lines mean
the concentration of the metal ions
what happens if there is more than one ion
the different wavelengths are put onto a single spectrum
what is flame emission spectroscopy an example of
an instrumental method