chemical analysis Flashcards
test for hydrogen
- squeaky pop test
1. remove bung and insert a burning splint
2. if hydrogen present it will pop
test for oxygen
- glowing splint
- place spring in test tube - if it relights oxygen is present
test for carbon dioxide?
- bubble gas through limewater
- repeat several times - if goes cloudy CO2 is present
chemical name for lime water
calcium hydroxide
test for chlorine?
- insert damp litmus paper into mouth of tube
- chlorine will bleach the paper and turn it white
how to carry out a flame test?
- place small amount of chemical onto wire mounted in a handle
- hold this over bunsen burner flame
what colour does lithium go when using flame tests?
crimson
what colour does sodium go when using flame tests?
yellow
what colour does potassium go when using flame tests?
lilac
what colour does calcium go when using flame tests?
orange-red
what colour does copper go when using flame tests?
green
what are the problems with flame tests?
colours difficult to distinguish
mixture of metals can mask colour of flame
how is flame emission spectroscopy carried out?
- sample of metal ion in solution is places in flame
- light given out is passed into a machine called spectroscope
- light is converted into light spectrum
- positions of lines are specific
how can we tell the concentration of an ion using flame emission spectroscopy?
the lines become more intense at a higher concentration
example of instrumental method
flame emission spectroscopy