CC2abcde Methods of Separating and Purifying Substances Flashcards

1
Q

The composition (make up) of a pure substances

A

Cannot be changed, is the same in all parts of a piece of the substance.

E.g Pure golf contains only gold atoms

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2
Q

State what is meant by the term ‘impure’

A

If a substance has more than one type of atom

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3
Q

Can compounds also be pure?

A

Yes

E.g. The sugar we use at home is a compound called sucrose. It contains carbon, hydrogen and oxygen atoms chemically bonded together to form sucrose molecules. You cannot change the composition of pure sucrose.

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4
Q

What is a mixture?

A

Contains elements and/or compounds that are chemically not joined together. You can use physical processes to separate mixtures into different substances.

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5
Q

Does a mixture have a fixed composition?

A

No

E.g. Air is a mixture of gases. When a student sits in a classroom, they use up oxygen and breathe out carbon dioxide and so the composition of the air in the room changes. We still call it ‘air’, but because air is a mixture its composition can change.

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6
Q

Describe how you would separate marbles from sand

A

Through the process of filtration.

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7
Q

What happens when a solid melts?

A

Its particles gain enough energy to overcome the weak forces of attraction between them. They move further away from one another and the solid becomes a liquid. The temperature at which this happens is called the melting point.

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8
Q

What is a physical property?

A

How a substance responds to forces and energy.

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9
Q

Will a pure substance melt the same way as an impure one?

A

No.
A pure substance has the same composition in every part of it, and so its physical properties are the same everywhere. So, all of the pure substance will melt at the same temperature until all the substance has changed state. A mixture can have different melting points.

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10
Q

List the ways in which pure substances are different from mixtures.

A

Pure - constant physical and chemical properties, sharp melting points, composition can’t be changes, made up of one element

Mixtures - impure, varied melting points, made up of more than 1 element

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11
Q

What is filtration?

A

Used to separate mixtures. They let smaller pieces or liquids through but trap bigger pieces or insoluble substances

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12
Q

What is a solution?

A

A mixture made of solutes (dissolved substances) in a liquid called the solvent.

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13
Q

What is crystalisation?

A

Solutes can be separated from a solution by evaporating the solvent to leave the solutes behind. The process forms solids crystals of various sizes. If the crystals form slowly, the particles have longer to form an ordered pattern and will make larger crystals.

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14
Q

Give one example of a mixture that can be separated by filtration.

A

Sand and water
Cereal and milk
Salt and sugar

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15
Q

Explain the process of filtration and crystallisation in the lab

A

To filter a solution, a filter funnel is lined with a filter paper that has fine holes in it. The solvent and solute pass through the fine holes to form the filtrate. Bits of insoluble substances cannot fit through the holes and so leave a residue in the filter paper. A Bunsen Burner is then used to evaporate the filtrate carefully. Care must be taken not to overheat the solution once it is saturated, because hot crystals may spit out. Further heating may also cause crystals to change chemically.

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16
Q

What can we do to reduce risks during experiments?

A
  • Wearing eye protection
  • Tying long hair back
  • Wearing heat prove gloves
  • Wearing a lab coat
  • Not drinking/eating
17
Q

Give names of two mixtures that can be separated by crystallisation

A
  • copper sulfate solution
  • salt solutions
18
Q

What is Chromatography?

A

Inks, paints and foods often contain mixtures of coloured compounds. Chromatography can be used to find out which coloured compounds the mixture contains.

19
Q

What requires expensive machinery in Chromatography?

A

The type of Chromatography used to analyse the substances in old oil paintings.

20
Q

What is Paper Chromatography?

A

A simpler technique that works because some compounds dissolve better in a solvent than others. When a solvent moves along the strip of paper, it carries the different substances in the mixture at different speeds, so they are separated. The solvent in called the mobile phase. The paper contains the stationary phase, though which the solvent and dissolved substances move. The paper with the separated components on it is called a chromatogram.

21
Q

What is the Rf value? How to calculate?

A

The distance the compound has risen / by the distance the solvent has risen.

Both measurements are made from the starting positions of the samples on the paper.

22
Q

What is Paper Chromatography used for?

A
  • To distinguish between pure and impure substances
  • To identify substances by comparing the pattern on the chromatogram which the patterns formed by known substances
  • To identify substances by calculating their Rf values
23
Q

What is distillation?

A

To make water pure we need to separate it from dissolved solids using distillation.

24
Q

How does a distillation apparatus work?

A

By heating a mixture of liquids to create vapor, which rises and is separated from the liquid. The vapor is then cooled and condensed, creating a separate liquid.

25
Q

What is fractional distillation?

A

Used to separate two or more liquids. This works because some liquids boil more easily than others. Liquids with lower boiling points evaporate more easily and will turn into vapour first.

26
Q

What is fractional distillation used for?

A
  • To separate the different products in crude oil
  • To make alcoholic drinks such as whiskey and vodka
  • To separate out the gases in the air, after the air has been cooled and turned into a liquid at -200ºC.
27
Q

Explain why a liquid with a lower boiling point will reach the top of a fractionating column more quickly than one with a higher boiling point.

A

They condense quicker their way to the top

28
Q

How does simple distillation work?

A

Water is heated so that vapour leaves quickly, then is cooled and condenses forming water without extra substances.