15. Finishing and Packaging Flashcards
Getting your wine ready for bottling day
What actions are done between 4-8 weeks bottling?
- Assemble final blend
- Full chemical analysis: alcohol, RS, free SO2 etc
Getting your wine ready for bottling day
What actions are done around 8 weeks before bottling day?
Final adjustments: alcohol, acidity, tannins if desired
Getting your wine ready for bottling day
What actions are done around 6 weeks before bottling day?
Protein stability trial and if necessary fine with bentonite
Getting your wine ready for bottling day
What actions are done between 4-6 weeks before bottling day?
Test for tartrate stability and, if necessary, treat
Getting your wine ready for bottling day
What actions are done around 4 weeks before bottling day?
Check protein stability and tartrate stability again, treat as necessary
Getting your wine ready for bottling day
What actions are done around 1-2 weeks before bottling day?
Add sweetening agents (eg RCGM) if using
Getting your wine ready for bottling day
What actions are done 72-48 hours before bottling?
Test filterability of the wine
Getting your wine ready for bottling day
What actions are done around 24 hours before bottling?
Adjust free SO2
Getting your wine ready for bottling day
What actions are done on bottling day?
Adjust dissolved oxygen and CO2
Getting your wine ready for bottling day
What actions need to be done during bottling?
Check dissolved oxygen (to ensure no pickup) and SO2 levels regularly and keep samples of bottled wines for quality assurance purposes
What is meant by sedimentation in post-fermentation clarification?
If the wine is stored in cool cellar conditions, suspended matter will gradually fall over time and form a sediment at the bottom of the container.
The wine can then be racked off, leaving the sediment behind.
What influences the number of rackings required to remove sedimentation?
- The shape and size of the container
- The volume of wine
- The available labour
Why do some producers choose only sedimentation to clarify their wine?
Some winemakers believe that clarification by sedimentation avoids the potential loss of texture and flavour that may occur if the wine is fined and filtered.
What are the costs associated with sedimentation as a clarification method?
- Labour
- Sedimentation takes time, prolonging the time before the wine can be bottled and released. However if the wine is to be barrel aged, then sedimentation happens during the barrel maturation process.
What is centrifugation?
This is a rapid process that spins the wine at high speed to clarify it. It can replace depth filtration and allow early bottling. It is very effective with wines with a lot of matter in suspension.
It is only practised in high-volume wineries to spread the considerable cost of buying the machine.
Name the three methods used to clarify the wine post-fermentation.
- Sedimentation
- Centriguation
- Fining
Producers typically use a combination of these methods, however some premium producers will only use sedimentation and racking.
What is fining?
Fining is a procedure in which a fining agent (protein or mineral origin) is added to speed up the process of the precipitation of suspended material in the wine.
Fining removes a small proportion of unstable colloids (microscopic particles too small to be removed by filtering) from the wine.
What is the difference between fining and filtration?
Fining is the addition of a fining agent to speed up the precipitation of suspended material in the wine. It can remove a portion of unstable colloids from the wine (where filtering cannot). Followed by racking.
Filtration is a physical separation technique used to eliminate solids from a suspension by passing it through a filter medium consisting of porous layers that trap solid particles, thus making the liquid clear.
Why do winemakers use fining as a technique to clarify their wines?
It helps to clarify the wine and to stabilise it against the formation of hazes later in the bottle.
Many fining agents are able to offer solutions to other problems, such as the removal of harsh tannins in red wines or browning in white wines.
What is an essential step before adding fining agents to the wine? Why?
- Winemakers conduct laboratory trials before using fining agents to ensure that the minimum effective amount is used.
- They then compare the fined sample with the original wine before proceeding.
- Many fining agents can remove desirable compounds from wine or make the wine unstable when too much is added (over-fining) and therefore it is important to add only the minimum effective amount.
What are the three categories of common fining agents?
- Those that remove unstable proteins
- Those that remove phenolics that contribute undesirable colour and bitterness
- Those that remove colour and off-odours.
How do fining agents work?
The fining agent must have the opposite charge from the wine colloid to be removed. The fining agent and the colloid attract each other and form a solid large enough to be removed by racking or by filtration.
What are colloids?
Microscopic particles too small to be removed by filtering
Why are white and rosé wines commonly fined with bentonite?
To remove grape-derived proteins that can agglomerate into a visible haze if warmed up (e.g. in transit). This can be seen as a fault.
Why is it not necessary to remove grape-derived proteins from red wine (by fining with bentonite)?
They bind with tannins, precipitate naturally and are removed when the wine is racked.
What is bentonite used for?
Bentonite is used as a fining agent to remove grape-derived, unstable proteins.
What is bentonite and how does it affect the wine?
- A form of clay that adsorbs unstable proteins and unstable colloidal colouring matter.
- It has a minimal effect on the flavour and texture of wine. It does lead to some colour loss in red wines and produces large amounts of sediment, and so wine is lost when it is racked off.
- Bentonite can be used to fine must as well as wine.
List six fining agents that remove phenolics that contribute undesirable colour and bitterness.
- Egg white
- Gelatine
- Casein
- Isinglass
- Vegetable protein products
- Polyvinylpolypyrrolidone (PVPPl)
These fining agents may be used in conjunction with bentonite for their own properties and to avoid risk of over-fining (which in itself could make the wine unstable).
What is a requirement when using egg whites as a fining agent?
As it is an allergen, it must be declared on the label if the wine is sold in the EU and other territories if present above a specified limit.
What kind of fining agent are egg whites typically used as?
Egg whites fall under the category of fining agents that remove phenolics that contrinute undesirable colour and bitterness.
Why are egg whites commonly used as a fining agent for high quality red wines?
It tends to be used for high-quality red wines because of its ability to remove harsh tannins and clarify wine. It is gentle to the wine.
What is gelatine and what is it used for?
A protein collagen extracted from pork that aids clarification, removes bitterness and astringency in red wine and browning in white wine pressings.
Fining agent (category 2)
What are the disadvantages to consider before using gelatine as a fining agent?
It must be added in the smallest effective amount as it is easy to over-fine with gelatine, stripping flavour and character, and creating the risk of a protein haze forming later.
It is not suitable for vegetarian or vegan wine as it is derived from animals.
What is casein?
Fining agent (category 2).
A milk-derived protein that removes browning from white wines and clarifies wines to some extent.
What is isinglass?
Fining agent category 2
A protein collagen derived from fish bladders that very effectively clarifies white wines, giving them a bright appearance.
What are the disadvantages of using isinglass as a fining agent?
The smallest effective amount must be added to avoid potential for the formation of a protein haze later and the creation of a fishy smell. It is not suitable for vegetarian or vegan wines as it is derived from fish bladders.
What is PVPP and what is it used for?
Polyvinylpolypyrrolidone is an insoluble plastic in powder form that removes browning and astringency from oxidised white wine. It is a gentler fining agent than charcoal. It is rarely used on red wines, but can reduce astringency and brighten the colour.
What are vegetable derived proteins, used as fining agents, made from?
Legumes or potatoes
What is charcoal used for in winemaking?
Charcoal is used as a fining agent that removes brown colours and off-odours.
What is the main risk of using charcoal as a fining agent? What can be done to mitigate this?
Care has to be taken as charcoal over-fines easily removing desirable aromas and flavours. One option is to treat only one batch of the affected wine and then blend it with the rest of the wine to reduce this effect.
What is filtration?
Filtration is a physical separation technique used to eliminate solids from a suspension by passing it through a filter medium consisting of porous layers that trap solid particles, thus making the liquid clear. Filtration is the most common way of clarifying wine.
What are the two main types of filtration?
Depth filtration
Surface filtration
What is depth filtration?
This method of filtration traps particles in the depth of the material that forms the filter
What are the advantages of depth filtration?
- It can cope with fluid with many particles in it; for example, wine that has just been pressed or lees.
- Does not block easily
Is depth filtration an absolute filter?
No.
If too much pressure is applied or if the filter is used for too long, some particles will make their way through the filter.
What is diatomaceous earth used for in winemaking?
Diatomaceous earth is used as a filter medium for depth filtration
What is the most common filter medium used in depth filtration?
Diamaceous earth
What is another term for diamaceous earth?
Kieselguhr
How is diamaceous earth used in depth filtration?
The DE is wetted and used as a filter medium. Wine is sucked by vacuum from the outside of a rotary drum, through the DE, to the inside of the drum.
Once the DE is processed, it is pure silica and inert.
What machinery can be used in depth filtration with diamaceous earth?
Rotary vauum filter (exposed to oxygen)
Enclosed DE filter (can be flushed with inert gases to avoid oxidation)
What is this?
Rotary vacuum filter with diamaceous earth stained with wine.
What type of filtration are rotary vacuum filters used for?
Depth filtration using diamaceous earth
Rotary vacuum filters use this method to filter very thick and cloudy wine (e.g. wine mixed with lees). It is an oxidative process as the drum is exposed to air.
Why might a winemaker choose to use an enclosed DE filter instead of a rotary vacuum filter?
Depth filtration with diamaceous earth
Enclosed DE filters can filter very thick and cloudy wine but can be flushed with an inert gas (e.g. nitrogen) to avoid oxidation taking place.
What are the costs associated with depth filtration using diamaceous earth?
- Inital investment of machinery
- Per litre cost of DE is small
- Skilled labour
- Used DE must be disposed of responsibly, which adds an additional cost.
Name two other terms for sheet filters.
Plate and frame filters
Pad filters
How do sheet filters work?
The wine is passed through a sheet of the filtering material. The more sheets there are in the filter, the quicker the wine can be filtered because any portion of wine only passes through one sheet. Very fine graded sheets can be used to remove any remaining yeasts at bottling.
What type of filtration method is sheet filtration?
Depth filtration
What two methods fall under the depth filtration category?
Diamaceous earth (using rotary vacuum filter or enclosed DE filter)
Sheet filters
What are the costs associated with sheet filters?
Sheet filter systems require investment initially (the frame must be very robust to withstand the pressures involved), although the cost of filter sheets is low. Trained personnel must operate them to work properly.
What are the two types of surface filters?
Membrane filters
Cross flow filters
What is the difference between depth filtration and surface filtration?
Depth filtration traps particles in the depth of the material that forms the filter (DE or sheet).
Surface filtration stops particles that are bigger than the pore size of the filter from going through. Known as an absolute filter.
What is this?
Sheet filter (depth filtration).
Why is depth filtration not considered an absolute filter?
They do not have a precisely defined pore size or structure whereas surface filtration does.
What is another term for membrane filters?
Cartridge filters
How do membrane filters work?
Membrane filters catch particles that will not go through the pore size of the filter.
What are the disadvantages of membrane filters?
They are slower than using a depth filter as the pores are smaller, often less than 1 micron. For the same reason, wine must be pre-filtered first (e.g. by depth filtration) as, otherwise, membrane filters can easily get blocked.
When are membrane filters usually used?
They are usually used as a final precaution immediately before the wine is bottled to ensure that the wine is completely clear with yeasts and bacteria removed and so it’s microbiologically stable (sterile filtration).
What does the term sterile filtration refer to?
Using membrane filtration systems as a final precaution to ensure the wine is completely clear of yeast and bacteria (therefore microbiologically stable) before bottling.
What are cross flow filters otherwise known as?
Tangential filters
How do cross flow filters work?
- The unfiltered wine passes through the filter, while also cleaning the surface of the filter, avoiding blockages.
- The filtered wine exits the filter, while the unfiltered wine passes through the filter again
- The result is completely filtered wine, with seperated solids.
What does the term stabilisation refer to?
The term ‘stabilisation’ is used to refer to several winemaking interventions which, if not carried out, could lead to undesired effects in the finished wine. This includes tackling the potential for unwanted hazes, deposits in the bottle and rapid changes in the wine (browning).
What is protein stabilisation?
The removal of grape-derived proteins that can create a haze in white and rosé wines after bottling (when the wine gets warm, eg transport).
Removed with bentonite as a fining agent
What are tartrates?
Tartrates, principally potassium bitartrate and, less frequently, calcium tartrate, are harmless deposits of crystals that can form in the finished wine.
What are the six techniques used for tartrate stability?
- Cold stabilisation
- Contact process
- Electrodialysis
- Ion exhange
- Carboxymethylcellulose (CMC)
- Metatartaric Acid
What fining agent is commonly used for protein stability?
Bentonite