Test 3 - Radioactivity Detectors Flashcards
C-14
5730 yrs, max E = 156 keV
H-3
12.4 yrs, max E = 19 keV
I-131
8.07 days, max E = 806 keV
I-125
60 days, max E = 35.49 keV
P-32
14.3 days, max E = 1709 keV
S-35
87.5 days, max E = 167 keV
Cl-36
3x10^5 years, max E = 709 keV
Liquid scintillation materials
- Emulsifying and aqueous - safer and organic. Scintillator & emulsifier.
- Organic and non-aqueous - organic aromatic solvent. Scintillator only.
Types of Quenching
Chemical, color, dilution, photon
Quenching
When competing radical-forming chemicals or photon-absorbing materials are present in the solution, or when photon escapes, quenching (incomplete transfer of energy) occurs.
Chemical quenching agents
Nitromethane, chloroform, carbon tetrachloride, acetone
DPM vs CPM
Decay per minute is a 100% efficient Counts per minute. Or, CPM x 100% / DPM = % counting efficiency.
LSC Advantage / Disadvantage
Advantage: small sample size okay, mixture of B distinguishable, short preparation. Disadvantage: expensive, bulky, and calibration required
Liquid scintillation counting
Technique of measuring photoelectron emission from beta source in liquid scintillator with two opposing PMT. Current in PMT corresponds to energy. Gamma source will not work (escapes easily).
Quench curve
Curve of CPM vs energy (so spectrum) with varying degrees of quenching. More quenching = lower counts.