Production Flashcards
Spirits
Spirits are defined as beverages in which the alcohol content has been concentrated by the process of distillation.
A spirit is the product of an initial fermentation followed by the distillation of that fermented liquid, resulting in a high-alcohol beverage.
Base Ingredients
Alcoholic spirits may be produced using a variety of different base ingredients
Depending on the choice of base ingredients, the production process of a spirit consists of either two or three main stages.
Base ingredients that contain readily available ingredients (honey, sugarcane, molasses, grapes, and fruits), only a two-stage production process is required.
Spirits produced from starchy materials (rice, potatoes, or grains) require a conversion process called saccharification.
Milling & Mash
Milling is the process of grinding and separating wheat and other cereal grains in preparation for malting.
*Mash is the mixture of base materials (typically ground malted and unmated grains mixed with water and cooked in a large cylindrical container called a mash tun) that is fermented into an alcoholic wash in preparation for production a spirit.
*Mash bill is the combination of grain used for mashing.
Fermentation
Fermentation is the action of yeast on the sugars in a solution – the yeast consumes and metabolizes the sugar, and in the process, converts the sugar into ethyl alcohol, carbon dioxide, and energy in the form of heat.
*After the fermentation is complete, the fermented liquid will have used up the yeast cells in the mixture (dead yeast cells are known as lees) – whole often discarded, there are times when the lees are used to impart additional flavor to a spirit.
Distillation
Once the initial fermentation is completed, the alcohol is concentrated to a desired degree using a spirit still.
Distillation is a complex process, but it’s based on one simple fact – alcohol has a lower boiling temperature than water, therefore the alcohol will dissipate into gas before the water begins to boil.
When the temperature reaches a point where the alcohol is above the boiling temperature (173 degrees Fahrenheit/78 degrees Celsius) the liquid will vaporize (turn to gas)
The vaporized alcohol and water are then captured in a closed vessel and cooled, the gasses will turn back into liquid and will have a higher concentration of alcohol than the original-water mixture.
Production
Saccharification
Milling
Milling is the process of grinding and separating wheat and other cereal grains in preparation for malting.
Mash
Mash is the mixture of base materials (typically ground malted and unmated grains mixed with water and cooked in a large cylindrical container called a mash tun) that is fermented into an alcoholic wash in preparation for production a spirit.
Boiling Points
The boiling point of a liquid is the highest temperature it may reach before it turns into gas.
Water vaporizes at 212 degrees Fahrenheit or 100 degrees Celsius.
Alcohol vaporized at 173 degrees Fahrenheit or 78 degrees Celsius.
Miscible Liquids
The boiling point of a liquid is the highest temperature it may reach before it turns into gas.
Water vaporizes at 212 degrees Fahrenheit or 100 degrees Celsius.
Alcohol vaporized at 173 degrees Fahrenheit or 78 degrees Celsius.
Fractional Distillation
Fractional distillation is the separation of a liquid mixture into fractions (components), separating chemical compounds by their boiling point and heating them to a temperature at which one or more fractions of the compound will vaporize.
Congeners
- Fractional distillation is the separation of a liquid mixture into fractions (components), separating chemical compounds by their boiling point and heating them to a temperature at which one or more fractions of the compound will vaporize.
Hearts
o The center part of the distillate or the potable spirit, this is the distiller’s main focus and this portion contains a variety of preferred congeners.
Heads
The first part of the distillate to come off, (also known as fore shots, contain compounds as low boilers (i.e., methanol-l and butyl alcohol) are are generally redistilled or discarded as many of these compounds are non-potable (not to be consumed without suffering adverse and undesirable effects.)
Tails
o The last part of the distillate which includes compounds called high boilers, which may be poisonous – typically distilled or discarded.
Post Distillation Processes:
Colorings and Other Additives
While many spirits get their color from the maturation process, other spirits are allowed to contain coloring agents.
Colors typically derived from caramel, which is added in order to create a consistently colored product.
Certain liqueurs and flavored spirits can be flavored post-distillation.
Bourbon whiskey is an example of a particular-distilled spirit for which it is illegal to add color agents.
Post Distillation Processes:
Filtration
Some spirits are filtered to remove any impurities, colors, or both
Filtration most commonly involves the use of activated charcoal, which absorbs the harasher characteristics of the spirit.
Filtration: Many spirits also undergo chill filtration because it removes components common to many spirits that can cause a spirit to be hazy or dull.
While the majority of matured spirits are chill filtered, typically those which are not will most often include either “non-chill filtered” or “un-chill filtered” on their labels.
During chill filtration, the spirit is chilled which causes congeners and fats to separate from the remaining spirit producing a hazy quality which can then be removed.
With all types of filtrations, precautions must be taken to avoid filtering out desirable components that contribute to body and flavor.
Post Distillation Processes:
Blending
In some cases, the finished spirit will be taken from a single batch or cask, but in many cases, the finished spirit will be a blend of many different batches and may be blended among multiple casks, ages, or even different distilleries.
The Master Blender’s role is crucial because the blending process helps maintain the house style of a particular spirit and allows the producer to create complexity and balance in the final spirit.
One notable exception to the practice of blending is the “single barrel” wherein one barrel is chosen from the distillery s inventory to be bottled without any blending taking place.
Post Distillation Processes:
Boiling Strength
Most spirits when taken off the still have an alcohol concentration of 58-96.5% by volume, which is generally reduced before bottling.
The process used to reduce the alcohol concentration after filtration and/or aging is referred to as “proofing” during which high-quality-water (often demineralized) or a mixture of water and spirit is added to the spirit.
For certain types of spirits, this process must be done very carefully and slowly to avoid a negative impact on the final product.
Some spirits that have matured for longer periods of time will lose alcohol strength naturally via evaporation and will not need dilution before bottling-.
It is common for “single barrel” whiskies to be bottled at cask strength which means that the proof of the spirit is extracted directly from the aged barrel.
Most spirits are bottled at 37-43% alcohol by volume.
Quercas Alba
American white oak, often used to mature spirits due to its abundance and its qualities and strength and reliance through the aging process and its ability to be shaped into a barrel.
Structural components of oak:
Cellulose:
An organic compound whose strength and chemical resistance provides structural integrity to the oak, permitting it to keep its shape and durability for years. (Makes up 40% of the mass of the wood)
- Hemicellulose:
An organic compound that is found in almost all plant cell walls and is composed of many different sugars with lower molecular weights than cellulose, which accounts for its easy solubility in alcohol – hemicellulose is responsible for the red layer that forms in charred oak barrels. (Makes up 25% of the mass of the wood).
- Lignin
The remaining 5-10% of the oak’s mass is comprised of tannins that are bitter and astringent (polyphenolic compounds) and small amounts of coconut flavored lactones and volatile phenolic acids. These acids are small in quantity but can provide over 400 aromatic and flavor combinations to the matured spirit.