Lab 12: Synthesis of Camphor Flashcards

1
Q

What common laundry solution was used inthe camphor experiment?

A

bleach

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2
Q

In the synthesis of camphor, what compound would be a common impurity?

A

isoborneol

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3
Q

What irritating, poisonous gas can be evolved during this reaction?

A

chlorine

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4
Q

What would be the characteristics of the melting point of your product if it were taken prior to sublimation?

A

the melting point would be lower and have a fairly broad melting point range

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5
Q

Assume you only allow 15 minute reaction period after the addition step in the camphor lab. How might this affect your product?

A

The yield and purity of camphor would be reduced

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6
Q

How do you eliminate excess HOCl at the end of the reaction in the camphor experiment?

A

Add sodium bisulfate as a reducing agent

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7
Q

WHich statement would correctly describe camphor?

A

a bridged bicyclic ketone

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8
Q

How might the IR of isoborneol differ from camphor?

A

isoborneol would show an OH stretch at 3600-3200cm-1

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9
Q

How many sp3 hybridized carbon atoms are found on a molecule of camphor?

A

9

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10
Q

Assume the reaction of isoborneol to camphor were reversed. What would the reaction be?

A

a reduction reaction

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