ICP-OES AAS Flashcards
Workflow of optical spectrometry : AA
Sample introduction –> Excitation source —> Spectrometer for wavelength —> Detector.
Flame AAS
-Single atomiser
- Dedicated flame
-Automatic gas box
-Standard and wide range PMT available
-Compatible with all other accessories
-Enhanced software as a standard
The AAS Optics
-Double beam optic
-Automatic
=wavelength
= Bandpass
= Slit height
=B/C on all system
- High D2 optical modulation
Stockdale optics
True double beam configuration with all of the drift correction advantages of that approach.
- We combine this stability with the optical energy efficiency benefits , and detection limit performance, of single beam design.
Thermal heating
Energy transferred through vessel then dissipated throughout the digestion.
Hot plate remains on after completion of the digestion, risk of heating to dryness
Microwave heating
-Vessel wall transparent to energy
-Direct activation of molecules in the solution
-Localized superheating maximizes heat transfer
-Upon reaction completion, energy addition stops, sealed container holds sample for when you are ready to work with it.