Chemistry practical = cracking Flashcards
Aim of this experiment
Catalytic cracking of long chain alkanes to shorter chain ones and alkenes
Step 1
Place mineral wool into boiling tube
Step 2
Add 2cm3 liquid paraffin into boiling tube so soaks into mineral wool
Remove excess paraffin
Step 3
Clamp boiling tube at the mouth at an angle
Step 4
Add aluminosilicate catalyst into tube
Ensure doesn’t fall to the bottom and touch the mineral wool and paraffin
What is good about the aluminosilicate in the middle of the tube?
Open structure so large surface area for reaction to take place on
Step 5
Attach bung with delivery tube to mouth of tube into a bowl of water with test tubes in water
Step 6
Use Bunsen flame to heat the catalyst stone
Briefly heat the paraffin
Step 7
Collect gas in test tube until many tubes are collected
Why is it important to always keep boiling tube hot?
By cooling, water may be sucked back into the boiling tube and then crack
So when finishing, remove from water first and ensure no water droplets are in the delivery tube and continue heating
Why is the boiling tube clamped at an angle?
To avoid the catalyst mixing with the paraffin
Why is the catalyst heated instead of the hydrocarbon?
Because then it would have evaporated without cracking