Chemical Analysis Flashcards
Chlorine test?
Hold damp litmus paper at the neck of a test tube, if chlorine is present, the damp litmus paper will be bleached by the chlorine
Oxygen test?
Hold a glowing splint at the neck of a test tube, if oxygen is present, it will relight
Hydrogen test?
Hold a lit splint at the neck of a test tube. If hydrogen is present, a squeaky pop sound is observed
Carbon dioxide test?
Bubble the gas being tested through lime water, if the gas is/contains CO2, the lime water will turn cloudy
How to carry out paper chromatography?
- Draw a line near the bottom of a sheet of paper
- use pencil as it is insoluble - Add a spot of ink the line using a capillary tube, and place the sheet in a beaker of solvent (water, ethanol…)
- make sure the ink isn’t touching the solvent so that it doesn’t dissolve in it - Optional - place a lid on the beaker to stop the solvent evaporating
- The solvent seeps up the paper, carrying the ink (solute) with it
- Each different dye in the ink will move up the paper at a different rate so the dyes will separate out. Each dye will form a spot in a different place
- When the solvent has nearly reached the top of the paper, remove it from the beaker and leave it to dry
- The end result is a pattern of spots called a chromatogram
What determines how far up the dyes travel up the paper?
The relative solubility of components making up a mixture determines how far they travel up the paper, The more soluble, the further it is carried
What is the mobile phase?
The mobile phase is the solvent that moves through the paper, carrying different substances with it
What is the stationary phase?
The stationary phase, is what the mobile phase moves through
What does it mean for a substance to be pure? examples
A substance made up of just 1 element or compound
- oxygen
- carbon dioxide
- distilled water
What is a mixture? examples
A mixture is a material made up of two or more different substances which are not chemically combined.
- air
- crude oil
- sea water
What is chromatography used for?
Chromatography is used to separate mixtures of substances into their components
What is simple distillation used for?
Simple distillation is used to separate a solvent from a solution
How does simple distillation work?
- The solution is heated. The part of the solution that has the lowest boiling point evaporates first
- The vapor is then cooled, condenses and collected
- The rest of the solution is left behind in the flask
What is the problem with simple distillation?
You can only use it to separate things with very different boiling points if the temperature goes higher than the boiling point of the substance with the higher boiling point, they will mix again.
What is fractional distillation used for?
To separate a mixture of liquids