Acids, Bases and Salt Preparations Flashcards
What is a salt
A salt is a metal compound formed when the H in the acid is replaced by a metal
What is the formula for ethanoic acid
CH3COOH
Which chlorides are insoluble
Silver chloride (AgCl)
Lead chloride (PbCl2)
Which sulfates are insoluble
Calcium sulfate
Barium sulfate
Lead sulfate
Which carbonates are insoluble
All of them, except sodium, potassium and ammonium
What are the three methods of preparing salts
Precipitation
Excess solid and acid
Titration
How do you determine which method to use when preparing a salt
If the salt is insoluble, then use precipitation
If the salt is soluble and has either sodium, potassium or ammonium ions then use titration
If the salt is soluble and does not have any sodium, potassium or ammonium ions, use the excess solid and acid method
Describe the process of precipitation
Mix the two solutions (one containing the cation and the other the anion) together in a beaker and stir with a glass rod until a precipitate forms. Separate the precipitate by filtration and then wash it with some distilled water. Lastly, dry it between two pieces of filter paper or in an over
What are the requirements for the excess solid and acid method
This method is used to prepare a soluble salt. One of the reactants MUST be insoluble. This means that it can be a metal (more reactive than hydrogen), a metal oxide, a metal hydroxide or a metal carbonate
Describe the excess solid and acid method
Add the solid to the hot dilute acid and stir until you can see it at the bottom of the beaker. Then, filter the mixture to remove any excess solid left and transfer the filtrate to an evaporating dish. There, heat it gently up to the point of crystallization until a saturated solution forms. Then, allow the solution to cool until crystals form and separate them by filtration. Lastly, rinse them with cold, distilled water and dry them between two pieces of filter paper
Describe the process of titration
For the experiment you will need an alkali and an acid ( e.g sodium hydroxide and hydrochloric acid). First, transfer 25cm of the acid into a conical flask using a pipette and add a few drops of phenolphthalein indicator. Then, fill the burette with the alkaline solution and slowly add it into the conical flask until the indicator changes color form colorless to pink. Record the volume of the solution added. Then, repeat the titration until two concordant titres are obtained and calculate the average titre using them. In a clean flask, add the average volume of the alkali found and 25cm of the acid without any indicator. Then, transfer the salt solution to an evaporating dish and heat it gently to evaporate the water up to the point of crystallization. Allow the saturated solution to cool and separate the crystals by filtration. Lastly, rinse them with a small amount of cold water and dry them between two pieces of filter paper